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C.Marthong / International Journal of Engineering Research and Applications
                    (IJERA)            ISSN: 2248-9622       www.ijera.com
                         Vol. 2, Issue4, July-August 2012, pp.1980-1985
          Sawdust Ash (SDA) as Partial Replacement of Cement
                                                C.Marthong
                    Lecturer, Civil Engineering Department, Shillong Polytechnic, Shillong
                                      Shillong, Meghalaya, India, 793008


ABSTRACT                                                  reaction [Meland, 1986]. Cement according to Shetty
         The possibility of using Sawdust Ash             [2005] is composed primarily of silica and lime,
(SDA) as a construction material was                      which form the essential cementing compounds
experimentally investigated. Saw dust was burnt           tricalcium (C3S) and dicalcium silicate (C2S). Any
and the ash sieved using a 90 micron sieve. Three         alteration in silica content will invariably affect the
grades of ordinary Portland cement (OPC)                  strength characteristics of cement, which is expected
namely; 33, 43 and 53 as classified by Bureau of          when SDA is used to partially replace with any
Indian Standard (BIS) are commonly used in                grades of cement for making concrete. The aimed of
construction industry. A comparative study on             this study is at sourcing of locally available material
effects of concrete properties when OPC of                for constructions in a bid to reduce the overall cost of
varying grades was partially replaced by SDA is           construction. Therefore, the present study cannot be
discussed in this paper. Percentage replacement of        underscored.
OPC with SDA was 0, 10, 20, 30 and 40%
respectively. Experimental investigations are             2. SAWDUST ASH (SDA)
carried out on mortar cubes, concrete cubes and                     Sawdust is an organic waste resulting from
beams specimens. The mix was designed for target          the mechanical milling or processing of timber
cube strength of 30 MPa at 28 days with water-            (wood) into various shapes and sizes. The dust is
cement ratio of 0.38. The compressive strength,           usually used as domestic fuel. The resulting ash
water absorption, shrinkage and durability of             known as saw-dust ash (SDA) is a form of pozzolana.
concrete were mainly studied. Test results shows          Dry sawdust concrete weighs only 30% as much as
that, inclusion of SDA cause little expansion due to      normal weight concrete and its insulating properties
low calcium content. Early strength development           approximate those of wood. With proper cement to
was observed to be about 50-60% of their 28 days          sawdust ratios, it is not flammable. As a basic
strength. The study suggests the use of SDA as            construction material, sawdust concrete does indeed
partial replacement of cement up to a maximum             have its functions. Sawdust is in abundance in North
of 10% by volume in all grades of cement.                 Eastern India (Meghalaya) and other parts of the
                                                          world. Experimental study to evaluate the behaviour
Keywords - Sawdust Ash, ordinary Portland                 of concrete properties both in plastic and hardened
cement (OPC), partial replacement.                        states with the inclusion of various waste products
                                                          such as fly ash [Naik and Ramme (1990),
1. INTRODUCTION                                           Gopalakrishna et al. (2001)], coconut ash [Oyelade
         According to American Society for Testing        and Akintoye (2011)], Rice hush ash [Nargale et al.,
Materials (ASTM, C-618-1978), pozzolana is a              2012] are available in the technical literature.
siliceous or a siliceous aluminous material which         Sawdust has been used in concrete for at least 30
contains little or no cementitious value, but in finely   years, but not widely. Although seriously limited by
divided form and in the presence of moisture or           its low compressive strength, sawdust concrete can
water, chemically reacts with calcium of moisture at      be made to perform well in certain floor and wall
ordinary temperature to form compound possessing          applications.
cementitious properties. Such material commonly                     Experimental investigation to evaluate the
includes fly ash, calcined diamotaceous earth, rice       possibility of using Sawdust Ash (SDA) as a
husk ash and pulverized burnt clay. Many researchers      construction material has been reported by Sumaila
are being done on the possible use of locally             and Job [1999], Udoeyo and Dashibil [2002].
available materials to partially replace cement in        Different grades of ordinary Portland cement (OPC)
concrete as cement is widely noted to be most             are available depending on the respective country
expensive constituents of concrete.                       codal classification. Bureau of Indian Standard (BIS)
         Extensive research has shown the use of          normally classify three grades of OPC namely: 33, 43
substitute’s material, which possessing pozzolanic        and 53, which are commonly used in construction
properties that it can produce concrete of better         industry. The possibility of using SDA as part
resistance to sulphate attack and reduce permeability.    replacement of OPC need to be investigate for
Mehta [1980] have shown that partial replacement of       confident used of these materials. The review of
cement by fly ash can also reduce heat of hydration.      literature however, could not find any comparative
Use of pozzolana can also reduce alkali aggregates        study on the effect of concrete properties when


                                                                                                 1980 | P a g e
C.Marthong / International Journal of Engineering Research and Applications
                    (IJERA)            ISSN: 2248-9622       www.ijera.com
                         Vol. 2, Issue4, July-August 2012, pp.1980-1985
cement of varying grades were partially replace by       salt concentration of sea water was considered. The
SDA are addressed together. Thus, in the present         specimens were alternately wetting and drying at 7
work a holistic approach was adopted to investigate      days intervals and then determining the strength loss
the possibility of using SDA as a construction           as a result of sulphate exposure for 28 days.
material. The contributions to strength gain,
improvement in durability, water absorption and
shrinkage are the main parameter of study.               Table 1: Physical and Chemical Properties of SDA
                                                                   and OPC
3. EXPERIMENTAL PROGRAM                                   Elements               SDA %       OPC % by
          Sawdust collected from local saw mill was                                 by          weight
used in this study. The sawdust was openly heated to                             weight
about the temperature of 600 ºC; the ash was then            Specific gravity      2.51     3.14 (33 OPC)
grounded after cooling and graded in accordance with                                        3.15 (43 OPC)
BS-812 [1967]. Chemical properties of SDA and                                               3.20 (53 OPC)
their comparison with OPC are presented in Table 1.       Moisture contents (%     2.16          0.344
          Coarse aggregate from crushed basalt rock            by weight)
was use. Flakiness and Elongation Index were                Loss on ignition       3.67           1.05
maintained well below 15 %. River sand was used as               (g/cm3)
fine aggregate. Material used have been tested as per               pH            11.12            12
relevant codal provision [IS 2386 (I, III), 1963]. The            SiO2            50.20          20.70
mix was designed for target cube strength of 30 MPa              AL2O3             1.02           5.75
at 28 days with water-cement ratio of 0.38. A simple              Fe2O3           14.23           2.50
method of mix proportioning using SDA (i.e. SDA as                CaO              5.45          64.00
part replacement of cement by weight) has been                    MgO              0.09           1.00
adopted. This was adopted due to remarkable                       MnO              5.60           0.05
difference in specific gravity of SDA and OPCs.                   Na2O             0.07           0.20
(SDA= 2.15, 33 OPC=3.14, 43 OPC=3.15 and 53
                                                                   K2O             9.57           0.60
OPC = 3.20)
                                                                  P2O5             0.56           0.15
          Various grades of ordinary Portland cement
(OPC) classified by BIS namely: 33, 43 and 53                      SO3             0.58           2.75
conforming to standard codal provision [IS 269-1989,
IS 8112-1989 and IS 12269-1987] were used. The
cement by SDA are 0, 10, 20, 30 and 40% per each         Table 2 Details of proportions of cement and fly ash
grades. Fly ash has been added as percentage by            Symbols        % of cement         % of SDA
weight of total cementitious material replacing             C100               100                 0
cement by various percentages. Table 2 illustrates the       F10                90                 10
detail of various percentages chosen.                        F20                80                 20
          Eighteen cubes of sizes 150x150x150 mm             F30                70                 30
were cast per variety of sample per each grades of           F40                60                 40
cement for strength test and water absorption test.
Cube strength was examined at different age’s i.e. 7,
28, 56 and 90 days. However, water absorption test       4. RESULTS AND DISCUSSION
were examined at 56 and 90 days. For water                         Various parameters which significantly
absorption, the cubes were kept moist for the above      affect the properties of concrete (plastic and harden
test age in tap water and then heated for 24 hours at    state) with the inclusion of SDA are discussed below.
110 ºC in an oven.
          Two un-reinforced beams of sizes 150           4.1 Effect of SDA on cementitious properties
x150x1000 mm per each grade of cement were cast                    The physical and chemical properties of
to measure the shrinkage. Shrinkage test of beam         SDA used in this study are shown in Table 1. It is
after 28 days of curing were done by measuring the       seen that the SDA proportion of silicon dioxide
change in length of the specimen at 7 days interval.     (SiO2), aluminum oxide (Al2O3) and iron oxide
Six mortar cubes of 50x50x50 mm were cast per            (Fe2O3) when combined together was 65.45%, which
variety of the sample and per each grades of cement      slightly less than that specified by ASTM C
for durability test (sulphate resistance). The           618[1978] for pozzolana but the average loss on
resistance to sulphate attack were evaluated by          ignition was 3.67 which satisfied the ASTM
immersion of well-cured specimens after 28 days of       requirement. The specific gravity of SDA was found
curing in a standard sodium sulphate solution            to be 2.51 which is about fourth-fifths that of cement
(Na2SO4) having concentration of 16 gm/l [Buenfeld       (33 OPC=3.14, 43 OPC=3.15 and 53 OPC = 3.20).
and Newman, 1984]. An enhanced sulphate salt             The pH value of SDA was evaluated as 11.12, which
concentration as high as eight times that of average     is alkaline in nature.

                                                                                              1981 | P a g e
C.Marthong / International Journal of Engineering Research and Applications
                                           (IJERA)            ISSN: 2248-9622       www.ijera.com
                                                Vol. 2, Issue4, July-August 2012, pp.1980-1985
The main physical properties of SDA that influence                        The variation of normal consistency for different
the activity in gaining strength is its fineness. SDA                     grades of OPC using different percentage SDA is
required having equal or finer than OPC for its good                      shown in Fig. 3. The plot indicates that the water
cementing efficiency. The fineness of the 33, 43 and                      requirement for the paste increases approximately
53 cement grades OPC in this investigation are found                      linearly for all grades of OPC. The normal
to be 9, 8 and 6% residue on 90 micron sieve size                         consistency of 43 and 53 grades cement are higher by
respectively. Fineness of SDA is found to be 5%.                          7 and 10% as compared to that of 33 grade cement.
This shows that SDA is of finer size as comparable to                     Further, the cement of 53 grades is finer as compared
cement particles. Thus, it is expected to have                            to 33 grades OPC; hence more water is required for
appreciable influence on the strength development on                      wetting the particles, as the total surface area of the
concrete.                                                                 particle is increases.
          The variation of setting time [initial setting
time (IST) and final setting time (FST)] and                                                       50




                                                                          Normal consistency (%)
soundness of OPCs and SDA are furnished in Fig. 1
                                                                                                   40
and 2 respectively. Fig. 1 shows that the setting time
increased with increasing SDA content. This                                                        30
behavior may be due to the low rate of hydration in
the paste containing SDA. Cement content is usually                                                20                 33 Grade OPC
accompanied by high rate of hydration and it is usual                                              10                 43 Grade OPC
that the reduction in cement content by replacing by                                                                  53 Grade OPC
SDA which is virtually inert at the early age would                                                0
be accompanied by a low heat of hydration. 33                                                           0      10       20       30        40          50
grades OPC takes longer time (both initial and final)                                                                   SDA (%)
as compared the other two grades. This same trend                                                       Fig. 3 Consistency with SDA content
was also observed by Marthong [2002] when OPC of
various grades were partially replaced by class-F fly                     4.2 Effect of SDA on concrete properties
ash. The soundness as shown in Fig. 2 slightly                            4.2.1 Workability
increased upon the inclusion of SDA. Soundness of                                  It was observed from the slump and
33 grades OPC was found to be slightly lower as                           compacting factors test that the slump decreased
compared to the other two grades of OPC. The                              upon the inclusion of SDA as partial replacement of
obtained values of setting time and soundness was                         OPC. Therefore, it can be inferred that to attain the
however, within the recommended range for all                             required workability, mixes containing SDA will
grades of OPC paste [IS 269-1989, IS 8112-1989 and                        required higher water content than the corresponding
IS 12269-1987].                                                           conventional mixes. The workability (slump) of
                                                                          concrete for 33, 43 and 53 grades OPC varies from
                 1200                   IST- 33 Grade OPC                 23, 18 and 10 mm for concrete containing 40% SDA
 Setting time (Min.)




                 1000                   IST- 43 Grade OPC                 respectively. The higher value of slump is obtained
                                        IST- 53 Grade OPC
                       800              FST-33 Grade OPC                  for concrete with cement of 33 grades and least for
                                        FST- 43 Grade OPC                 53 grades cement. This behaviour was as expected
                       600              FST- 53 Grade OPC                 because higher the grade of cement the more fine it
                       400                                                is. Finer cement requires more water to wet the
                       200                                                surface particles.
                         0                                                4.2.2 Compressive strength
                              0        10      20      30       40   50            The Variation of cubes strength at different
                                              SDA (%)                     ages of 7, 28, 56 and 90 days with different grades of
                             Fig. 1 Setting times with SDA content        OPC and various percentage of SDA contents are
                                                                          shown in Fig. 4 to 6. The figure indicates that
                         3                                                compressive strength of concrete in all grades of
                                                                          OPC at early age is significantly higher than that of
        Soundness (mm)




                                                                          concrete produced with SDA. It was also observed
                         2
                                                                          that compressive strength continued to increase with
                                                                          age but decreased with SDA contents in all grades of
                                       33 Grade OPC                       OPC. The reduction in strength at the initial stages of
                         1             43 Grade OPC                       hydration may be because SDA acts as a retarder.
                                       53 Grade OPC
                                                                          The initial processes of hydration get retarded, which
                         0                                                invariably may affect the initial process of strength
                             0        10      20       30       40   50   development. The strength reduction was found to be
                                              SDA (%)                     lower for higher grade OPC. Comparison on the
                              Fig. 2 Soundness with SDA content           attaining of strength at 28 days it was observed SDA

                                                                                                                                      1982 | P a g e
C.Marthong / International Journal of Engineering Research and Applications
                                     (IJERA)            ISSN: 2248-9622       www.ijera.com
                                          Vol. 2, Issue4, July-August 2012, pp.1980-1985
with 43 and 53 grades OPC attained about 60% of                       4.2.3 Water absorption
strength as compared to normal concrete, while SDA                              The water absorption was calculated on the
with 33 grades OPC could attain only 50% of its                       basis of initial soaked cube and then oven dried. Fig.
strength. This comparison shows that SDA 43 and 53                    7 shows the variation in water absorption with SDA
OPC with medium workability concrete compared                         contents. The test results depict that water absorption
favorably with OPC concrete in term of early                          up to 20% replacement decreased with the inclusion
strength development. In long term strength gain (at                  of SDA in all grades OPC as compared to pure
90 days), SDA 43 and 53 grades OPC attained about                     cement and there after start increasing. The water
80% strength as compared to concrete with 0% SDA                      absorption of 53 grade OPC concrete with SDA
replacement, while SDA 33 grades OPC the strength                     content is least than the other two and being
gain was about 58% only. The comparison clearly                       maximum for 33 grades OPC concrete. This
shows that strength of SDA concrete slightly increase                 behaviour may be due to the fact that, 53 grade
with age in all three grades of OPCs. Thus it indicate                cement is finer and 33 grade OPC being coarser
that replacement by SDA for 43 and 53 grades OPC                      particles. Thus, permeability of paste with coarser
is seems to be better in term of ultimate strength gain               cement particle is higher. The water absorption of
than that of 33 grades OPC. The same behavior was                     SDA concrete also varies with age of concrete. The
also observed by Marthong [2002] when OPC of                          results also depict that water absorption too decreased
various grades were partially replaced by class-F fly                 with age. With age the water absorption decreased
ash. However, the optimum strength of SDA concrete                    because gel gradually fills the original water filled
was observed to be 10% replacement in all the three                   spaces.
grades of OPCs.
                                                                                             12          33 Grade OPC-56 days
                                                                      Water absorption (%)
                  50                                                                                     43 Grade OPC-56 days
                                                       7 Days                                10
                                                                                                         53 Grade OPC-56 days
 Strength (MPa)




                  40                                   28 Days                                           33 Grade OPC-90 days
                                                                                             8
                                                       56 Days                                           43 Grade OPC-90 days
                  30                                                                         6           53 Grade OPC-90 days
                  20                                                                         4
                  10                                                                         2
                  0                                                                          0
                       0       10      20     30      40        50                                0     10      20       30        40      50
                                      SDA (%)                                                                   SDA (%)
                  Fig. 4 Compressive strength of 33 grade OPC                                 Fig. 7 Water absorption with SDA content

                  50                                                  4.2.4 Shrinkage
                                                       7 Days                  It is well know that shrinkage directly relate
 Strength (MPa)




                  40                                   28 Days
                                                                      to consistency. The consistency of SDA cementitious
                                                       56 Days
                  30                                                  paste decreased as compared to OPC cement paste.
                                                                      This shows that shrinkage should decreased in SDA
                  20                                                  concrete due to the reduction in water demand and
                  10                                                  production of finer paste structure, which restrict the
                                                                      loss of pore water within the paste. However, in the
                   0                                                  present study it has been observed that the shrinkage
                       0       10      20     30      40         50   of specimens with 40% SDA content measured at the
                                      SDA (%)                         age of 90 days found to be same for pure and SDA
                  Fig. 5 Compressive strength of 43 grade OPC         concrete at each proportion. This is in line with the
                                                                      observation by Marthong [2002] when OPC of
                  50                                                  various grades were partially replaced by class-F fly
                                                       7 Days         ash. Hence, it may be concluded that influence of
                                                       28 Days
 Strength (MPa)




                  40                                                  SDA on shrinkage is negligible.
                                                       56 Days
                  30
                                                                      4.2.5 Durability
                  20                                                           Variation in compressive strength with SDA
                                                                      content for 28 days exposed in sulphate solution and
                  10                                                  tap-water are shown in Fig. 8. The figure
                   0                                                  demonstrates that, for each grades of cement the
                                                                      strength of ordinary cube and that partially replaced
                       0        10     20     30      40         50
                                     SDA (%)                          by SDA immersed in sulphate solution have less
                  Fig. 6 Compressive strength of 53 grade OPC         compressive strength than the corresponding referral

                                                                                                                              1983 | P a g e
C.Marthong / International Journal of Engineering Research and Applications
                                    (IJERA)            ISSN: 2248-9622       www.ijera.com
                                         Vol. 2, Issue4, July-August 2012, pp.1980-1985
cubes immersed in tap-water. Strength decreases as                     5. Water absorption of SDA concrete up to 20%
SDA contents increases. The decreased in cube                             replacement decreased with the increased in
strength exposed in sulphate solution over that                           grades of OPC.
exposed in tap-water are about 8% for ordinary cubes                   6. Shrinkage of SDA concrete is similar to the pure
and that of 40% SDA content are about 10-20% for                          cement concrete in all grades of OPC.
all grades of OPC. Thus, inclusion of SDA as partial                   7. Inclusion of SDA as partial replacement of
replacement of cement seems that it does not improve                      cement does not improve the durability when
the durability when exposed to sulphate environment.                      exposed to sulphate environment. However, SDA
Comparing all the three grades of OPC, the strength                       with 53 grades OPC seems to be better.
loss seem to be betters for 53 grade OPC as
compared to the other two grades.
                 40                                                    REFERENCES
                                                                        [1]  ASTM. Specification for pozzolanas. ASTM
                                                                             C 618 1978, Philadelphi.
                 30                                                     [2]  N. R. Buenfeld and J.B. Newman. The
Strength (MPa)




                                                                             permeability of concrete in marine
                                                                             environment. Magazine of concrete research,
                 20           33 Grade OPC exposed in tap-water
                                                                             Vol. 36, 1984, pp. 67.
                              43 Grade OPC exposed in tap water
                              53 Grade OPC exposed in tap-water         [3]  British Standard Institution. Methods for
                              33 Grade OPC exposed in Sulphate soln.         sampling and testing of mineral aggregate,
                 10                                                          Sands and Fillers, BS. 812, 1967.
                              43 Grade OPC exposed in Sulphate soln.
                              53 Grade OPC exposed in Sulphate soln.    [4]  S. Gopalakrishna, N. P. Rajamane, M.
                                                                             Neelamegam, J. A. Peter and and J. K.
                 0
                                                                             Dattatreya. Effect of partial replacement of
                      0       10       20       30      40       50          cement with fly ash on the strength and
                                    SDA (%)                                  durability of HPC. The Indian Concrete
                  Fig. 8 Compressive strength under different                Journal, 2001, pp. 335-341.
                                environment                             [5]  IS: 2386-1963. Methods of test for
                                                                             aggregates for concrete - Part 1: Particle
                                                                             size and shape. Bureau of Indian Standard,
5. CONCLUSIONS                                                               New Delhi.
         From the experimental work carried out and                     [6]  IS 2386-1963. Methods of Test for
the analysis of the results following conclusions seem                       aggregates for concrete - Part 3: Specific
to be valid for possible use of SDA as partial                               gravity, Density, Voids, Absorption and
replacement of cement.                                                       Bulking. Bureau of Indian Standard, New
1. Important oxides content was 65.45% by weight                             Delhi.
   of SDA and has a pH value of 11.12, which shows                      [7]  IS 269-1989. Specification for OPC-33
   that it’s alkaline in nature. This shows that SDA                         grade cement. Bureau of Indian Standard,
   has a significant physical and chemical property                          New Delhi.
   that encourages its uses as a pozzolanas.                            [8]  IS 8112-1989. Specification for OPC-43
2. Setting times increased in all grades of OPC upon                         grade cement. Bureau of Indian Standard,
   the addition of SDA but are in the range                                  New Delhi.
   recommended for pure cement.                                         [9]  IS 12269-1987. Specification for OPC-53
3. Workability decreased upon the inclusion of SDA.                          grade cement. Bureau of Indian Standard,
   Thus, mixes containing SDA will required higher                           New Delhi.
   water content than the corresponding conventional                    [10] P. K. Mehta. Performance tests for sulphate
   mixes.                                                                    resistance and alkali silica reactivity of
4. Compressive strength of concrete increases with                           hydraulic cement. Durability of building
   grade of cement. Early strength development was                           components. ASTM STP 691, ASTM
   observed to be about 50-60% of their 28 days                              Philadelphia, 1980, pp. 336-345.
   strength. Test results indicate that SDA concrete                    [11] F. Meland. Use of fly ash in cement to
   can attain the same order of strength as                                  reduce alkali-silica reaction. Fly ash, silica
   conventional concrete at longer curing periods.                           fume, slag and natural pozzolana in
   The rate of strength gain by SDA-33 grades OPC                            concrete. Pro. 2nd Int. Conf: ACI pub. Sp-91,
   is lower as compared to 43 and 53 grades.                                 V.M.Malhotra, ed., American Concrete
   However, study suggested the use of SDA as                                Institute (ACI), Detroit, Mich., 1986, pp.
   partial replacement of cement up to a maximum                             591-608.
   of 10% by volume in all grades of cement.                            [12] C. Marthong. Effect of partial replacement
                                                                             of three grades of cement by fly ash on
                                                                             concrete properties. M.Tech Thesis, Civil

                                                                                                           1984 | P a g e
C.Marthong / International Journal of Engineering Research and Applications
                  (IJERA)            ISSN: 2248-9622       www.ijera.com
                       Vol. 2, Issue4, July-August 2012, pp.1980-1985
       Engineering Department, Institute of
       Technology-BHU, 2002, Varanasi, India.
[13]    T. R. Naik and B. W. Ramme. Effects of
       highlime. Fly ash content on water demand,
       time of set and compressive strength of
       concrete. ACI Materials Journal, 87, 1990,
       pp. 619-26.
[14]    S. D. Nagrale, H. Hajare and P. R. Modak.
       Utilization of Rice Husk Ash. International
       Journal of Engineering Research and
       Applications (IJERA) Vol. 2(4), 2012, pp. 1-
       5.
[15]    F. F. Oyelade and O. Akintoye. Coconut
       Husk Ash as a Partial Replacement of
       Cement in Sandcrete Block Production. Pro.
       11th Int. Conf. and 32nd Annual General
       Meeting of the Nigerian Institution of
       Agricultural Engineers. October 17 – 20,
       2011, Ilorin, Nigeria.
[16]    M. S. Shetty. Concrete Technology. S.
       Chand & Company Ltd., 2005, New Delhi.
[17]    S. A. Sumaila and O. F. Job. Properties of
       SDA-OPC        concrete:    A    preliminary
       assessment. Journal of Environmental
       Science. Vol.3 (2), 1999, pp. 155-159.
[18]    F. F. Udoeyo and P. U. Dashibil. Sawdust
       Ash as Concrete Material. Journal of
       Materials in Civil Engineering. ASCE, Vol.
       14(2):               2002,              173.




                                                                              1985 | P a g e

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Lw2419801985

  • 1. C.Marthong / International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622 www.ijera.com Vol. 2, Issue4, July-August 2012, pp.1980-1985 Sawdust Ash (SDA) as Partial Replacement of Cement C.Marthong Lecturer, Civil Engineering Department, Shillong Polytechnic, Shillong Shillong, Meghalaya, India, 793008 ABSTRACT reaction [Meland, 1986]. Cement according to Shetty The possibility of using Sawdust Ash [2005] is composed primarily of silica and lime, (SDA) as a construction material was which form the essential cementing compounds experimentally investigated. Saw dust was burnt tricalcium (C3S) and dicalcium silicate (C2S). Any and the ash sieved using a 90 micron sieve. Three alteration in silica content will invariably affect the grades of ordinary Portland cement (OPC) strength characteristics of cement, which is expected namely; 33, 43 and 53 as classified by Bureau of when SDA is used to partially replace with any Indian Standard (BIS) are commonly used in grades of cement for making concrete. The aimed of construction industry. A comparative study on this study is at sourcing of locally available material effects of concrete properties when OPC of for constructions in a bid to reduce the overall cost of varying grades was partially replaced by SDA is construction. Therefore, the present study cannot be discussed in this paper. Percentage replacement of underscored. OPC with SDA was 0, 10, 20, 30 and 40% respectively. Experimental investigations are 2. SAWDUST ASH (SDA) carried out on mortar cubes, concrete cubes and Sawdust is an organic waste resulting from beams specimens. The mix was designed for target the mechanical milling or processing of timber cube strength of 30 MPa at 28 days with water- (wood) into various shapes and sizes. The dust is cement ratio of 0.38. The compressive strength, usually used as domestic fuel. The resulting ash water absorption, shrinkage and durability of known as saw-dust ash (SDA) is a form of pozzolana. concrete were mainly studied. Test results shows Dry sawdust concrete weighs only 30% as much as that, inclusion of SDA cause little expansion due to normal weight concrete and its insulating properties low calcium content. Early strength development approximate those of wood. With proper cement to was observed to be about 50-60% of their 28 days sawdust ratios, it is not flammable. As a basic strength. The study suggests the use of SDA as construction material, sawdust concrete does indeed partial replacement of cement up to a maximum have its functions. Sawdust is in abundance in North of 10% by volume in all grades of cement. Eastern India (Meghalaya) and other parts of the world. Experimental study to evaluate the behaviour Keywords - Sawdust Ash, ordinary Portland of concrete properties both in plastic and hardened cement (OPC), partial replacement. states with the inclusion of various waste products such as fly ash [Naik and Ramme (1990), 1. INTRODUCTION Gopalakrishna et al. (2001)], coconut ash [Oyelade According to American Society for Testing and Akintoye (2011)], Rice hush ash [Nargale et al., Materials (ASTM, C-618-1978), pozzolana is a 2012] are available in the technical literature. siliceous or a siliceous aluminous material which Sawdust has been used in concrete for at least 30 contains little or no cementitious value, but in finely years, but not widely. Although seriously limited by divided form and in the presence of moisture or its low compressive strength, sawdust concrete can water, chemically reacts with calcium of moisture at be made to perform well in certain floor and wall ordinary temperature to form compound possessing applications. cementitious properties. Such material commonly Experimental investigation to evaluate the includes fly ash, calcined diamotaceous earth, rice possibility of using Sawdust Ash (SDA) as a husk ash and pulverized burnt clay. Many researchers construction material has been reported by Sumaila are being done on the possible use of locally and Job [1999], Udoeyo and Dashibil [2002]. available materials to partially replace cement in Different grades of ordinary Portland cement (OPC) concrete as cement is widely noted to be most are available depending on the respective country expensive constituents of concrete. codal classification. Bureau of Indian Standard (BIS) Extensive research has shown the use of normally classify three grades of OPC namely: 33, 43 substitute’s material, which possessing pozzolanic and 53, which are commonly used in construction properties that it can produce concrete of better industry. The possibility of using SDA as part resistance to sulphate attack and reduce permeability. replacement of OPC need to be investigate for Mehta [1980] have shown that partial replacement of confident used of these materials. The review of cement by fly ash can also reduce heat of hydration. literature however, could not find any comparative Use of pozzolana can also reduce alkali aggregates study on the effect of concrete properties when 1980 | P a g e
  • 2. C.Marthong / International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622 www.ijera.com Vol. 2, Issue4, July-August 2012, pp.1980-1985 cement of varying grades were partially replace by salt concentration of sea water was considered. The SDA are addressed together. Thus, in the present specimens were alternately wetting and drying at 7 work a holistic approach was adopted to investigate days intervals and then determining the strength loss the possibility of using SDA as a construction as a result of sulphate exposure for 28 days. material. The contributions to strength gain, improvement in durability, water absorption and shrinkage are the main parameter of study. Table 1: Physical and Chemical Properties of SDA and OPC 3. EXPERIMENTAL PROGRAM Elements SDA % OPC % by Sawdust collected from local saw mill was by weight used in this study. The sawdust was openly heated to weight about the temperature of 600 ºC; the ash was then Specific gravity 2.51 3.14 (33 OPC) grounded after cooling and graded in accordance with 3.15 (43 OPC) BS-812 [1967]. Chemical properties of SDA and 3.20 (53 OPC) their comparison with OPC are presented in Table 1. Moisture contents (% 2.16 0.344 Coarse aggregate from crushed basalt rock by weight) was use. Flakiness and Elongation Index were Loss on ignition 3.67 1.05 maintained well below 15 %. River sand was used as (g/cm3) fine aggregate. Material used have been tested as per pH 11.12 12 relevant codal provision [IS 2386 (I, III), 1963]. The SiO2 50.20 20.70 mix was designed for target cube strength of 30 MPa AL2O3 1.02 5.75 at 28 days with water-cement ratio of 0.38. A simple Fe2O3 14.23 2.50 method of mix proportioning using SDA (i.e. SDA as CaO 5.45 64.00 part replacement of cement by weight) has been MgO 0.09 1.00 adopted. This was adopted due to remarkable MnO 5.60 0.05 difference in specific gravity of SDA and OPCs. Na2O 0.07 0.20 (SDA= 2.15, 33 OPC=3.14, 43 OPC=3.15 and 53 K2O 9.57 0.60 OPC = 3.20) P2O5 0.56 0.15 Various grades of ordinary Portland cement (OPC) classified by BIS namely: 33, 43 and 53 SO3 0.58 2.75 conforming to standard codal provision [IS 269-1989, IS 8112-1989 and IS 12269-1987] were used. The cement by SDA are 0, 10, 20, 30 and 40% per each Table 2 Details of proportions of cement and fly ash grades. Fly ash has been added as percentage by Symbols % of cement % of SDA weight of total cementitious material replacing C100 100 0 cement by various percentages. Table 2 illustrates the F10 90 10 detail of various percentages chosen. F20 80 20 Eighteen cubes of sizes 150x150x150 mm F30 70 30 were cast per variety of sample per each grades of F40 60 40 cement for strength test and water absorption test. Cube strength was examined at different age’s i.e. 7, 28, 56 and 90 days. However, water absorption test 4. RESULTS AND DISCUSSION were examined at 56 and 90 days. For water Various parameters which significantly absorption, the cubes were kept moist for the above affect the properties of concrete (plastic and harden test age in tap water and then heated for 24 hours at state) with the inclusion of SDA are discussed below. 110 ºC in an oven. Two un-reinforced beams of sizes 150 4.1 Effect of SDA on cementitious properties x150x1000 mm per each grade of cement were cast The physical and chemical properties of to measure the shrinkage. Shrinkage test of beam SDA used in this study are shown in Table 1. It is after 28 days of curing were done by measuring the seen that the SDA proportion of silicon dioxide change in length of the specimen at 7 days interval. (SiO2), aluminum oxide (Al2O3) and iron oxide Six mortar cubes of 50x50x50 mm were cast per (Fe2O3) when combined together was 65.45%, which variety of the sample and per each grades of cement slightly less than that specified by ASTM C for durability test (sulphate resistance). The 618[1978] for pozzolana but the average loss on resistance to sulphate attack were evaluated by ignition was 3.67 which satisfied the ASTM immersion of well-cured specimens after 28 days of requirement. The specific gravity of SDA was found curing in a standard sodium sulphate solution to be 2.51 which is about fourth-fifths that of cement (Na2SO4) having concentration of 16 gm/l [Buenfeld (33 OPC=3.14, 43 OPC=3.15 and 53 OPC = 3.20). and Newman, 1984]. An enhanced sulphate salt The pH value of SDA was evaluated as 11.12, which concentration as high as eight times that of average is alkaline in nature. 1981 | P a g e
  • 3. C.Marthong / International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622 www.ijera.com Vol. 2, Issue4, July-August 2012, pp.1980-1985 The main physical properties of SDA that influence The variation of normal consistency for different the activity in gaining strength is its fineness. SDA grades of OPC using different percentage SDA is required having equal or finer than OPC for its good shown in Fig. 3. The plot indicates that the water cementing efficiency. The fineness of the 33, 43 and requirement for the paste increases approximately 53 cement grades OPC in this investigation are found linearly for all grades of OPC. The normal to be 9, 8 and 6% residue on 90 micron sieve size consistency of 43 and 53 grades cement are higher by respectively. Fineness of SDA is found to be 5%. 7 and 10% as compared to that of 33 grade cement. This shows that SDA is of finer size as comparable to Further, the cement of 53 grades is finer as compared cement particles. Thus, it is expected to have to 33 grades OPC; hence more water is required for appreciable influence on the strength development on wetting the particles, as the total surface area of the concrete. particle is increases. The variation of setting time [initial setting time (IST) and final setting time (FST)] and 50 Normal consistency (%) soundness of OPCs and SDA are furnished in Fig. 1 40 and 2 respectively. Fig. 1 shows that the setting time increased with increasing SDA content. This 30 behavior may be due to the low rate of hydration in the paste containing SDA. Cement content is usually 20 33 Grade OPC accompanied by high rate of hydration and it is usual 10 43 Grade OPC that the reduction in cement content by replacing by 53 Grade OPC SDA which is virtually inert at the early age would 0 be accompanied by a low heat of hydration. 33 0 10 20 30 40 50 grades OPC takes longer time (both initial and final) SDA (%) as compared the other two grades. This same trend Fig. 3 Consistency with SDA content was also observed by Marthong [2002] when OPC of various grades were partially replaced by class-F fly 4.2 Effect of SDA on concrete properties ash. The soundness as shown in Fig. 2 slightly 4.2.1 Workability increased upon the inclusion of SDA. Soundness of It was observed from the slump and 33 grades OPC was found to be slightly lower as compacting factors test that the slump decreased compared to the other two grades of OPC. The upon the inclusion of SDA as partial replacement of obtained values of setting time and soundness was OPC. Therefore, it can be inferred that to attain the however, within the recommended range for all required workability, mixes containing SDA will grades of OPC paste [IS 269-1989, IS 8112-1989 and required higher water content than the corresponding IS 12269-1987]. conventional mixes. The workability (slump) of concrete for 33, 43 and 53 grades OPC varies from 1200 IST- 33 Grade OPC 23, 18 and 10 mm for concrete containing 40% SDA Setting time (Min.) 1000 IST- 43 Grade OPC respectively. The higher value of slump is obtained IST- 53 Grade OPC 800 FST-33 Grade OPC for concrete with cement of 33 grades and least for FST- 43 Grade OPC 53 grades cement. This behaviour was as expected 600 FST- 53 Grade OPC because higher the grade of cement the more fine it 400 is. Finer cement requires more water to wet the 200 surface particles. 0 4.2.2 Compressive strength 0 10 20 30 40 50 The Variation of cubes strength at different SDA (%) ages of 7, 28, 56 and 90 days with different grades of Fig. 1 Setting times with SDA content OPC and various percentage of SDA contents are shown in Fig. 4 to 6. The figure indicates that 3 compressive strength of concrete in all grades of OPC at early age is significantly higher than that of Soundness (mm) concrete produced with SDA. It was also observed 2 that compressive strength continued to increase with age but decreased with SDA contents in all grades of 33 Grade OPC OPC. The reduction in strength at the initial stages of 1 43 Grade OPC hydration may be because SDA acts as a retarder. 53 Grade OPC The initial processes of hydration get retarded, which 0 invariably may affect the initial process of strength 0 10 20 30 40 50 development. The strength reduction was found to be SDA (%) lower for higher grade OPC. Comparison on the Fig. 2 Soundness with SDA content attaining of strength at 28 days it was observed SDA 1982 | P a g e
  • 4. C.Marthong / International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622 www.ijera.com Vol. 2, Issue4, July-August 2012, pp.1980-1985 with 43 and 53 grades OPC attained about 60% of 4.2.3 Water absorption strength as compared to normal concrete, while SDA The water absorption was calculated on the with 33 grades OPC could attain only 50% of its basis of initial soaked cube and then oven dried. Fig. strength. This comparison shows that SDA 43 and 53 7 shows the variation in water absorption with SDA OPC with medium workability concrete compared contents. The test results depict that water absorption favorably with OPC concrete in term of early up to 20% replacement decreased with the inclusion strength development. In long term strength gain (at of SDA in all grades OPC as compared to pure 90 days), SDA 43 and 53 grades OPC attained about cement and there after start increasing. The water 80% strength as compared to concrete with 0% SDA absorption of 53 grade OPC concrete with SDA replacement, while SDA 33 grades OPC the strength content is least than the other two and being gain was about 58% only. The comparison clearly maximum for 33 grades OPC concrete. This shows that strength of SDA concrete slightly increase behaviour may be due to the fact that, 53 grade with age in all three grades of OPCs. Thus it indicate cement is finer and 33 grade OPC being coarser that replacement by SDA for 43 and 53 grades OPC particles. Thus, permeability of paste with coarser is seems to be better in term of ultimate strength gain cement particle is higher. The water absorption of than that of 33 grades OPC. The same behavior was SDA concrete also varies with age of concrete. The also observed by Marthong [2002] when OPC of results also depict that water absorption too decreased various grades were partially replaced by class-F fly with age. With age the water absorption decreased ash. However, the optimum strength of SDA concrete because gel gradually fills the original water filled was observed to be 10% replacement in all the three spaces. grades of OPCs. 12 33 Grade OPC-56 days Water absorption (%) 50 43 Grade OPC-56 days 7 Days 10 53 Grade OPC-56 days Strength (MPa) 40 28 Days 33 Grade OPC-90 days 8 56 Days 43 Grade OPC-90 days 30 6 53 Grade OPC-90 days 20 4 10 2 0 0 0 10 20 30 40 50 0 10 20 30 40 50 SDA (%) SDA (%) Fig. 4 Compressive strength of 33 grade OPC Fig. 7 Water absorption with SDA content 50 4.2.4 Shrinkage 7 Days It is well know that shrinkage directly relate Strength (MPa) 40 28 Days to consistency. The consistency of SDA cementitious 56 Days 30 paste decreased as compared to OPC cement paste. This shows that shrinkage should decreased in SDA 20 concrete due to the reduction in water demand and 10 production of finer paste structure, which restrict the loss of pore water within the paste. However, in the 0 present study it has been observed that the shrinkage 0 10 20 30 40 50 of specimens with 40% SDA content measured at the SDA (%) age of 90 days found to be same for pure and SDA Fig. 5 Compressive strength of 43 grade OPC concrete at each proportion. This is in line with the observation by Marthong [2002] when OPC of 50 various grades were partially replaced by class-F fly 7 Days ash. Hence, it may be concluded that influence of 28 Days Strength (MPa) 40 SDA on shrinkage is negligible. 56 Days 30 4.2.5 Durability 20 Variation in compressive strength with SDA content for 28 days exposed in sulphate solution and 10 tap-water are shown in Fig. 8. The figure 0 demonstrates that, for each grades of cement the strength of ordinary cube and that partially replaced 0 10 20 30 40 50 SDA (%) by SDA immersed in sulphate solution have less Fig. 6 Compressive strength of 53 grade OPC compressive strength than the corresponding referral 1983 | P a g e
  • 5. C.Marthong / International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622 www.ijera.com Vol. 2, Issue4, July-August 2012, pp.1980-1985 cubes immersed in tap-water. Strength decreases as 5. Water absorption of SDA concrete up to 20% SDA contents increases. The decreased in cube replacement decreased with the increased in strength exposed in sulphate solution over that grades of OPC. exposed in tap-water are about 8% for ordinary cubes 6. Shrinkage of SDA concrete is similar to the pure and that of 40% SDA content are about 10-20% for cement concrete in all grades of OPC. all grades of OPC. Thus, inclusion of SDA as partial 7. Inclusion of SDA as partial replacement of replacement of cement seems that it does not improve cement does not improve the durability when the durability when exposed to sulphate environment. exposed to sulphate environment. However, SDA Comparing all the three grades of OPC, the strength with 53 grades OPC seems to be better. loss seem to be betters for 53 grade OPC as compared to the other two grades. 40 REFERENCES [1] ASTM. Specification for pozzolanas. ASTM C 618 1978, Philadelphi. 30 [2] N. R. Buenfeld and J.B. Newman. The Strength (MPa) permeability of concrete in marine environment. Magazine of concrete research, 20 33 Grade OPC exposed in tap-water Vol. 36, 1984, pp. 67. 43 Grade OPC exposed in tap water 53 Grade OPC exposed in tap-water [3] British Standard Institution. Methods for 33 Grade OPC exposed in Sulphate soln. sampling and testing of mineral aggregate, 10 Sands and Fillers, BS. 812, 1967. 43 Grade OPC exposed in Sulphate soln. 53 Grade OPC exposed in Sulphate soln. [4] S. Gopalakrishna, N. P. Rajamane, M. Neelamegam, J. A. Peter and and J. K. 0 Dattatreya. Effect of partial replacement of 0 10 20 30 40 50 cement with fly ash on the strength and SDA (%) durability of HPC. The Indian Concrete Fig. 8 Compressive strength under different Journal, 2001, pp. 335-341. environment [5] IS: 2386-1963. Methods of test for aggregates for concrete - Part 1: Particle size and shape. Bureau of Indian Standard, 5. CONCLUSIONS New Delhi. From the experimental work carried out and [6] IS 2386-1963. Methods of Test for the analysis of the results following conclusions seem aggregates for concrete - Part 3: Specific to be valid for possible use of SDA as partial gravity, Density, Voids, Absorption and replacement of cement. Bulking. Bureau of Indian Standard, New 1. Important oxides content was 65.45% by weight Delhi. of SDA and has a pH value of 11.12, which shows [7] IS 269-1989. Specification for OPC-33 that it’s alkaline in nature. This shows that SDA grade cement. Bureau of Indian Standard, has a significant physical and chemical property New Delhi. that encourages its uses as a pozzolanas. [8] IS 8112-1989. Specification for OPC-43 2. Setting times increased in all grades of OPC upon grade cement. Bureau of Indian Standard, the addition of SDA but are in the range New Delhi. recommended for pure cement. [9] IS 12269-1987. Specification for OPC-53 3. Workability decreased upon the inclusion of SDA. grade cement. Bureau of Indian Standard, Thus, mixes containing SDA will required higher New Delhi. water content than the corresponding conventional [10] P. K. Mehta. Performance tests for sulphate mixes. resistance and alkali silica reactivity of 4. Compressive strength of concrete increases with hydraulic cement. Durability of building grade of cement. Early strength development was components. ASTM STP 691, ASTM observed to be about 50-60% of their 28 days Philadelphia, 1980, pp. 336-345. strength. Test results indicate that SDA concrete [11] F. Meland. Use of fly ash in cement to can attain the same order of strength as reduce alkali-silica reaction. Fly ash, silica conventional concrete at longer curing periods. fume, slag and natural pozzolana in The rate of strength gain by SDA-33 grades OPC concrete. Pro. 2nd Int. Conf: ACI pub. Sp-91, is lower as compared to 43 and 53 grades. V.M.Malhotra, ed., American Concrete However, study suggested the use of SDA as Institute (ACI), Detroit, Mich., 1986, pp. partial replacement of cement up to a maximum 591-608. of 10% by volume in all grades of cement. [12] C. Marthong. Effect of partial replacement of three grades of cement by fly ash on concrete properties. M.Tech Thesis, Civil 1984 | P a g e
  • 6. C.Marthong / International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622 www.ijera.com Vol. 2, Issue4, July-August 2012, pp.1980-1985 Engineering Department, Institute of Technology-BHU, 2002, Varanasi, India. [13] T. R. Naik and B. W. Ramme. Effects of highlime. Fly ash content on water demand, time of set and compressive strength of concrete. ACI Materials Journal, 87, 1990, pp. 619-26. [14] S. D. Nagrale, H. Hajare and P. R. Modak. Utilization of Rice Husk Ash. International Journal of Engineering Research and Applications (IJERA) Vol. 2(4), 2012, pp. 1- 5. [15] F. F. Oyelade and O. Akintoye. Coconut Husk Ash as a Partial Replacement of Cement in Sandcrete Block Production. Pro. 11th Int. Conf. and 32nd Annual General Meeting of the Nigerian Institution of Agricultural Engineers. October 17 – 20, 2011, Ilorin, Nigeria. [16] M. S. Shetty. Concrete Technology. S. Chand & Company Ltd., 2005, New Delhi. [17] S. A. Sumaila and O. F. Job. Properties of SDA-OPC concrete: A preliminary assessment. Journal of Environmental Science. Vol.3 (2), 1999, pp. 155-159. [18] F. F. Udoeyo and P. U. Dashibil. Sawdust Ash as Concrete Material. Journal of Materials in Civil Engineering. ASCE, Vol. 14(2): 2002, 173. 1985 | P a g e