Butter: Manufacturing Process and Standard specifications

P
PRASANNA BHALERAOPhD Scholar en Institute of Chemical Technology, Mumbai
Butter Definition
As per FSSAI (2011)
Butter means the fatty product derived exclusively from milk of
cow and/or buffalo or its products principally in the form of water-
in-oil type of an emulsion.
Characteristics:
• Product may be with or without added Preservative (Common salt),
starter cultures of harmless lactic acid and/or flavour producing bacteria
and Colouring matter (Annato and Carotene).
• It should be free from animal oil, wax, and mineral oil.
• It shall have pleasant taste, free from off flavour and rancidity.
• It shall conform to the microbiological requirements of the regulation.
FSSAI standards for butter
Product Moisture Milk Fat Milk solids
not fat
Common
salt
Table
Butter
16.0%
(w/w, max.)
80.0%
(w/w, min.)
1.5% (w/w,
max.)
3.0% (w/w,
max.)
Desi butter --- 76.0%
(w/w, min.)
--- ---
Permitted food additives in
butter as per FSSAI
Additive Quantity
Colours (natural: singly or in combination)
Curcumin 100 ppm max
Beta carotene 100 ppm max
Carotene (natural extract) 100 ppm max
Annatto extract on bixin/nor bixin basis
(50:50)
20 pm max
Beta apo-8 carotenal 35 ppm max
Methyl ester of beta apo-8 carotenoic acid 35 ppm max
Acidity regulators
Sodium and calcium hydroxide 2000 ppm max
Microbiological
requirements of butterMicrobiological
parameters
Count
Total plate count
10,000/g
50,000/g
Coliform count
10/g
50/g
E.coli Absent/g
Salmonella Absent/g
Staphylococcus aureus
10/g
50/g
Yeast and mould count
20/g
50/g
Listeria monocytogenes Absent/g
Butter Definition
As per CODEX
Butter is a fatty product derived exclusively from milk and/or
products obtained from milk, principally in the form of an emulsion
of the type water-in-oil.
Permitted ingredients:
• Sodium chloride and food grade salt
• Starter cultures of harmless lactic acid and/or flavour producing
bacteria
• Potable water.
Butter Composition
As per CODEX
Minimum milk fat content 80%
Maximum water content 16%
Maximum milk solids-not-fat (SNF) content 2%
Based on
acidity of
cream
Based on
salt content
Based on
end use
Based on the
MFG
practice
CLASSIFICATION OF BUTTER
Based on acidity
of cream
Sweet cream butter
Mildly acidified
butter
Sour cream butter
CLASSIFICATION OF BUTTER
Non-acidified cream;
pH of ≥6.4
partially acidified
sweet cream,
pH 5.2 to 6.3.
ripened cream
>0.2% acidity
pH ≤ 5.1.
Based on salt
content :
Salted butter
Unsalted butter
CLASSIFICATION OF BUTTER
Improved flavour and
keeping quality
Used for preparation
of ghee and butter oil
Based on end use
Table Butter
White Butter
CLASSIFICATION OF BUTTER
Salt and Colour
(Annato/ Carotene),
Flavour (Diacetyl)
No preservatives
Made from pasteurized cream obtained from cow or buffalo milk
with combination of above ingredients
Based on the
manufacturing
practice
Pasteurized
Cream/Table
Butter
Desi Butter
CLASSIFICATION OF BUTTER
Made from
Pasteurized Sweet
Cream
Made by churning of
Dahi/ Malai
Followed by FSSAI (2011).
Butter Manufacturing Process
Contd....
Pasteuriuzation (82-88˚C)
Standardization (35-40% fat)
Neutralization
Seperation
Preheating (35-40˚C)
Grading, Weighing, Sampling
Receiving of milk
Storage (-23 to -29˚C)
Packaging
Salting
Churning
Cooling and Ageing (5-10˚C)
Ripening (20-22˚C)
Grading of Cream
Grading
1st Grade Cream
(Sweet/ Slightly
Sour)
2nd Grade Cream
(Sour,
Coagulated)
Rejected Cream
(Markedly sour,
fermented)
Objectives of neutralization
1. To reduce the acidity in cream to a point (0.14 -0.16%) which
permits pasteurization without risk of curdling,
2. To produce butter which can be kept well in cold storage
3. To avoid excess loss of fat which result from the churning
cream i.e. excessively sour.
4. To prevent undesirable flavors which may result when a
cream of high acid which is subjected for pasteurization at
higher temperatures.
5. To improve the keeping quality of butter from high acid
cream. Salted-acid-butter develops a fish flavor during
commercial storage at -23 to -29°C.
Factors affecting neutralization
• Accurate neutralization of sour cream is important to get a
desired quality product.
a. Accuracy in sampling.
b. Accuracy in testing.
c. Accuracy in estimation of amounts of cream and neutralizer.
d. Careful weighing the quantity of neutralizer.
e. Thorough mixing of neutralizer in cream prior to
pasteurization.
Methods of neutralization of
cream
• There are five essential steps to follow for cream
neutralization. These are:
1. Adoption of definite standard of churning acidity
2. Correct estimation of acidity
3. Calculating the amount of neutralizer to be added
4. Adding neutralizer in the correct manner
5. Checking results by re-testing acidity
Types of Neutralizers
• The neutralizers used for reducing acidity in cream.
 Lime Neutralizers
 Soda Neutralizers
Lime Neutralizers
• The neutralizers used for
reducing acidity in cream.
• Types:
1. Low magnesium limes
(<5% Lime)
2. Medium magnesium
limes (30-35%)
3. High magnesium limes
(45 to 55% )
Soda Neutralizers
• Bicarbonate of soda or
baking soda are used.
Types of Neutralizers
Standardization of Cream
• Adjustment of fat to desired level.
• Pearson square method is used.
• Done by adding calculated quantity of skim milk or butter
milk.
• Desired level of fat in cream for butter making is 33 to 40%
• Standardization to both higher and lower level leads to
higher fat loss in butter milk.
Pasteurization of Cream
• Adjustment every particle of cream to a temperature not less
that 71°C and holding it at that temperature for at least 20 min
or any suitable temperature-time combination using properly
operated equipment.
• A number of equipment can be employed for this purpose.
• More severe heat treatment of cream should be avoided
• Pasteurization of cream for making ripened cream butter is
commonly carried out at higher temperature than for sweet
cream butter e.g. 90-95ºC for 15 or 105-110ºC with no
holding.
Ripening of Cream
• Main object of cream ripening is to produce butter with higher
di-acetyl content.
• Starter culture consisting of a mixture of:
1. Acid producing: (Streptococcus lactis, S.cremories)
2. Flavour producing: (S.diacetylactis, L.citrovorum and
L.dextranicum)
• Amount of starter added usually ranges between 0.5-2.0% of
the weight of the cream
• After thoroughly mixed, the cream is incubated at about
21°C till desired an acidity is reached.
Contd.....
• Cream is subsequently cooled to 5-10°C to arrest further acid
development.
• Biosynthesis of diacetyl is not sufficient above pH 5.2.
• Stopping fermentation of cream by cooling at pH 5.1-5.3,
results in a milder flavour; whereas continuing fermentation
up to pH 4.5-4.7 results in higher levels of both diacetyl and
lactic acid, giving more pronounced flavour
Cooling and Ageing
• When cream leaves the pasteurizer, the fat in the globule is in liquid
form.
• When cream is cooled, fat crystallization starts, cream will not churn
unless the butter fat is at least partially crystallized.
• If solidification of fat is not sufficient, the fat losses in butter are
high.
• The temperature to which cream is cooled is chosen is such a way
that the butter produced is of optimum consistency and cream
churns to butter in a responsible time of about 35-45 minutes.
• Churning at too high temperature may give butter with ‘greasy‘
body which may work up too quickly and become sticky.
• Generally cooling temperature in summer should be 7-9°C and that
of in winter 10-13°C.
CHURNING OF CREAM
 Churning is initiated by agitation of cream causing
incorporation of numerous air bubbles into the cream.
 With incorporation of air there is increase in the volume of
cream and air plasma interface.
 Surface active (such as frictional, impact, concussion etc.)
causes partial disruption of fat globule membrane
 The fat film, thus formed, serve as a foam depressant causing
the air bubble to burst.
 The liquid fat also serves as cementing material causing fat
globules to clump together and eventually butter grains are
formed which floats in plasma i.e. butter milk.
Initial Working
• Working of butter is essentially a kneading process in which
butter granules are formed into a compact mass.
• During this operation, any excess moisture or buttermilk is
removed.
• However, the emulsion (w/o) at this stage is not fully stable.
Salting of Butter
• In conventional process, butter may be salted by adding salt to
butter churn after initial working of butter.
• Salt sets up osmotic gradient which draws water from the
butter grains. This can lead butter to be leaky.
• Salt may be added either in dry form or as saturated brine
solution.
Packaging and Storage
• Stored at -23 to -29oC.
• Moisture proof or grease proof wrappers are used for
packaging.
• Overrun in butter:
• The weight of butter obtained from a given lot of cream
exceeds the amount of fat in the cream. That amount of butter
which exceeds the fat present in cream is called as overrun.
Butter: Manufacturing Process and Standard specifications
1 de 28

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Butter: Manufacturing Process and Standard specifications

  • 1. Butter Definition As per FSSAI (2011) Butter means the fatty product derived exclusively from milk of cow and/or buffalo or its products principally in the form of water- in-oil type of an emulsion. Characteristics: • Product may be with or without added Preservative (Common salt), starter cultures of harmless lactic acid and/or flavour producing bacteria and Colouring matter (Annato and Carotene). • It should be free from animal oil, wax, and mineral oil. • It shall have pleasant taste, free from off flavour and rancidity. • It shall conform to the microbiological requirements of the regulation.
  • 2. FSSAI standards for butter Product Moisture Milk Fat Milk solids not fat Common salt Table Butter 16.0% (w/w, max.) 80.0% (w/w, min.) 1.5% (w/w, max.) 3.0% (w/w, max.) Desi butter --- 76.0% (w/w, min.) --- ---
  • 3. Permitted food additives in butter as per FSSAI Additive Quantity Colours (natural: singly or in combination) Curcumin 100 ppm max Beta carotene 100 ppm max Carotene (natural extract) 100 ppm max Annatto extract on bixin/nor bixin basis (50:50) 20 pm max Beta apo-8 carotenal 35 ppm max Methyl ester of beta apo-8 carotenoic acid 35 ppm max Acidity regulators Sodium and calcium hydroxide 2000 ppm max
  • 4. Microbiological requirements of butterMicrobiological parameters Count Total plate count 10,000/g 50,000/g Coliform count 10/g 50/g E.coli Absent/g Salmonella Absent/g Staphylococcus aureus 10/g 50/g Yeast and mould count 20/g 50/g Listeria monocytogenes Absent/g
  • 5. Butter Definition As per CODEX Butter is a fatty product derived exclusively from milk and/or products obtained from milk, principally in the form of an emulsion of the type water-in-oil. Permitted ingredients: • Sodium chloride and food grade salt • Starter cultures of harmless lactic acid and/or flavour producing bacteria • Potable water.
  • 6. Butter Composition As per CODEX Minimum milk fat content 80% Maximum water content 16% Maximum milk solids-not-fat (SNF) content 2%
  • 7. Based on acidity of cream Based on salt content Based on end use Based on the MFG practice CLASSIFICATION OF BUTTER
  • 8. Based on acidity of cream Sweet cream butter Mildly acidified butter Sour cream butter CLASSIFICATION OF BUTTER Non-acidified cream; pH of ≥6.4 partially acidified sweet cream, pH 5.2 to 6.3. ripened cream >0.2% acidity pH ≤ 5.1.
  • 9. Based on salt content : Salted butter Unsalted butter CLASSIFICATION OF BUTTER Improved flavour and keeping quality Used for preparation of ghee and butter oil
  • 10. Based on end use Table Butter White Butter CLASSIFICATION OF BUTTER Salt and Colour (Annato/ Carotene), Flavour (Diacetyl) No preservatives Made from pasteurized cream obtained from cow or buffalo milk with combination of above ingredients
  • 11. Based on the manufacturing practice Pasteurized Cream/Table Butter Desi Butter CLASSIFICATION OF BUTTER Made from Pasteurized Sweet Cream Made by churning of Dahi/ Malai Followed by FSSAI (2011).
  • 12. Butter Manufacturing Process Contd.... Pasteuriuzation (82-88˚C) Standardization (35-40% fat) Neutralization Seperation Preheating (35-40˚C) Grading, Weighing, Sampling Receiving of milk Storage (-23 to -29˚C) Packaging Salting Churning Cooling and Ageing (5-10˚C) Ripening (20-22˚C)
  • 13. Grading of Cream Grading 1st Grade Cream (Sweet/ Slightly Sour) 2nd Grade Cream (Sour, Coagulated) Rejected Cream (Markedly sour, fermented)
  • 14. Objectives of neutralization 1. To reduce the acidity in cream to a point (0.14 -0.16%) which permits pasteurization without risk of curdling, 2. To produce butter which can be kept well in cold storage 3. To avoid excess loss of fat which result from the churning cream i.e. excessively sour. 4. To prevent undesirable flavors which may result when a cream of high acid which is subjected for pasteurization at higher temperatures. 5. To improve the keeping quality of butter from high acid cream. Salted-acid-butter develops a fish flavor during commercial storage at -23 to -29°C.
  • 15. Factors affecting neutralization • Accurate neutralization of sour cream is important to get a desired quality product. a. Accuracy in sampling. b. Accuracy in testing. c. Accuracy in estimation of amounts of cream and neutralizer. d. Careful weighing the quantity of neutralizer. e. Thorough mixing of neutralizer in cream prior to pasteurization.
  • 16. Methods of neutralization of cream • There are five essential steps to follow for cream neutralization. These are: 1. Adoption of definite standard of churning acidity 2. Correct estimation of acidity 3. Calculating the amount of neutralizer to be added 4. Adding neutralizer in the correct manner 5. Checking results by re-testing acidity
  • 17. Types of Neutralizers • The neutralizers used for reducing acidity in cream.  Lime Neutralizers  Soda Neutralizers
  • 18. Lime Neutralizers • The neutralizers used for reducing acidity in cream. • Types: 1. Low magnesium limes (<5% Lime) 2. Medium magnesium limes (30-35%) 3. High magnesium limes (45 to 55% ) Soda Neutralizers • Bicarbonate of soda or baking soda are used. Types of Neutralizers
  • 19. Standardization of Cream • Adjustment of fat to desired level. • Pearson square method is used. • Done by adding calculated quantity of skim milk or butter milk. • Desired level of fat in cream for butter making is 33 to 40% • Standardization to both higher and lower level leads to higher fat loss in butter milk.
  • 20. Pasteurization of Cream • Adjustment every particle of cream to a temperature not less that 71°C and holding it at that temperature for at least 20 min or any suitable temperature-time combination using properly operated equipment. • A number of equipment can be employed for this purpose. • More severe heat treatment of cream should be avoided • Pasteurization of cream for making ripened cream butter is commonly carried out at higher temperature than for sweet cream butter e.g. 90-95ºC for 15 or 105-110ºC with no holding.
  • 21. Ripening of Cream • Main object of cream ripening is to produce butter with higher di-acetyl content. • Starter culture consisting of a mixture of: 1. Acid producing: (Streptococcus lactis, S.cremories) 2. Flavour producing: (S.diacetylactis, L.citrovorum and L.dextranicum) • Amount of starter added usually ranges between 0.5-2.0% of the weight of the cream • After thoroughly mixed, the cream is incubated at about 21°C till desired an acidity is reached.
  • 22. Contd..... • Cream is subsequently cooled to 5-10°C to arrest further acid development. • Biosynthesis of diacetyl is not sufficient above pH 5.2. • Stopping fermentation of cream by cooling at pH 5.1-5.3, results in a milder flavour; whereas continuing fermentation up to pH 4.5-4.7 results in higher levels of both diacetyl and lactic acid, giving more pronounced flavour
  • 23. Cooling and Ageing • When cream leaves the pasteurizer, the fat in the globule is in liquid form. • When cream is cooled, fat crystallization starts, cream will not churn unless the butter fat is at least partially crystallized. • If solidification of fat is not sufficient, the fat losses in butter are high. • The temperature to which cream is cooled is chosen is such a way that the butter produced is of optimum consistency and cream churns to butter in a responsible time of about 35-45 minutes. • Churning at too high temperature may give butter with ‘greasy‘ body which may work up too quickly and become sticky. • Generally cooling temperature in summer should be 7-9°C and that of in winter 10-13°C.
  • 24. CHURNING OF CREAM  Churning is initiated by agitation of cream causing incorporation of numerous air bubbles into the cream.  With incorporation of air there is increase in the volume of cream and air plasma interface.  Surface active (such as frictional, impact, concussion etc.) causes partial disruption of fat globule membrane  The fat film, thus formed, serve as a foam depressant causing the air bubble to burst.  The liquid fat also serves as cementing material causing fat globules to clump together and eventually butter grains are formed which floats in plasma i.e. butter milk.
  • 25. Initial Working • Working of butter is essentially a kneading process in which butter granules are formed into a compact mass. • During this operation, any excess moisture or buttermilk is removed. • However, the emulsion (w/o) at this stage is not fully stable.
  • 26. Salting of Butter • In conventional process, butter may be salted by adding salt to butter churn after initial working of butter. • Salt sets up osmotic gradient which draws water from the butter grains. This can lead butter to be leaky. • Salt may be added either in dry form or as saturated brine solution.
  • 27. Packaging and Storage • Stored at -23 to -29oC. • Moisture proof or grease proof wrappers are used for packaging. • Overrun in butter: • The weight of butter obtained from a given lot of cream exceeds the amount of fat in the cream. That amount of butter which exceeds the fat present in cream is called as overrun.