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Heartfelt Greetings on
Silver Wedding Anniversary
From :
PRINCIPAL
&
STAFF
MEMBERS

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Synthesis and Characterization of 2,2-Biimidazole Complexes of Oxocations of Molybdenum (VI, V) and Uranium(VI) To cite this article: Samir S. Kandil & Loutfy H. Madkour (1993) Synthesis and Characterization of 2,2-Biimidazole Complexes of Oxocations of Molybdenum (VI, V) and Uranium(VI), Spectroscopy Letters: An International Journal for Rapid Communication, 26:3, 535-550, DOI: 10.1080/00387019308011552 To link to this article: http://dx.doi.org/10.1080/00387019308011552 2,2.-Biimidazole complexes of Moo2 , Moo2+ and U02f2 have been prepared and characterized by elemental analysis, conductance; and 'H NMR, IR and electronic spectra. Two types of complexes have been identified. Those obtained from slightly acidic solutions have the formulae MOO 22 (H bim)C12.2H20 'l, U02(H2bim)(Ac)2 2 and U02(H2bim)C12.2H20 whereas those from alkaline solutions have the formulae M0~0~(Hbim)~.2H~O 4, and M02(Hbim)2 (M = Mo(V1) 5, U(V1) 6). The infrared spectra of these complexes show characteristic biimidazole frequencies in the 3200-2500, 1550-1000 and 150 cm-l regions as well as metal oxygen double bonds in the 900 cm-l region. complex has been confirmed from 'H NMR signal ratios of The stoichiometries of the acetate biimidazole to acetate protons at 7.3 and 2.3 ppm, respec- tively. The electronic spectrum of molybdenum(V) complex showed d-d transition band at =13,500 cm-' in accord with that' reported for copper (d ) imidazole complexes; as well as peaks due to charge transfer bands at 30,000-26,000 c9-l. Peaks assignable to BIM --+ U(V1) were located at ~26,600 cm . The most probable structures of these complexes have been suggested.

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