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Estimation of Temperature
 Distribution in Silicon during Micro
      Laser Assisted Machining
                                Presented by
                               Kamlesh Suthar
                                     John Patten*
                             Western Michigan University
                         Manufacturing Engineering Department
                             Kalamazoo, MI-49008, USA
                Lei Dong                                     Hisham Abdel-Aal
           Condor USA, Inc.                         Department of General Engineering
8318 Pineville-Matthews Road, Suite 276             University of Wisconsin at Platteville
         Charlotte, NC-28226                            Platteville, WI- 53818, USA
Outline
                               Objective
                                                Analytical       Finite Element
                        Experimental work
                                                Modeling            Analysis
                       • Tool               • Point heat       • Gaussian Profile
                         Modification         source             heat source
                       • Measurement of     • Plane Heat
                         laser power          source
                       • Characterization   • Gaussian Beam
                                              Laser Heat
                         • AFM
                                              Source
                         • Thermal
                           imaging



                                                              Summary

                                                                                    2
MSEC-2008 ASME Conference, Evanston, IL
Motivation
     • Semiconductor and ceramic materials are
       highly brittle and plastic deformation at room
       temperature is difficult and they prone to
       fracture during machining
     • Brittleness has detrimental effect on tool
     • Therefore, the challenge is to develop a cost
       effective machining process which can
       produce ultra fine surface finish

                                                        3
MSEC-2008 ASME Conference, Evanston, IL
Objective
   • Silicon is highly brittle at room temperature and the
     hardness is the function of temperature
   • High Pressure Phase Transformation (HPPT) is one
     of the process mechanisms involved in ductile
     machining of semiconductors and ceramics.
   • Preferentially heat the HPPT material to increase
     ductility through thermal softening
           – Reduce tool wear
           – Minimize surface and subsurface damage.
   • Thermal Softening temperature for silicon is 600-
     800 oC
                                                         4
MSEC-2008 ASME Conference, Evanston, IL
Effect of Temperature on Hardness of
               Silicon




     (Trefilov,1963)
                                       5
Schematic of -LAM of Silicon




                                               6
MSEC-2008 ASME Conference, Evanston, IL
Diamond Tip Attachment




                                                                           250 um

                                                                                          90 Conical Tip
                                                                                          5 μm radius

                  Attachment was done at Digital Optical Company (Charlotte, NC) by Jay Matthews




                                                                                                        7
MSEC-2008 ASME Conference, Evanston, IL
Deliverable Power After Attachment
                                of Diamond & Laser Parameter
                                        Laser (0~400mw,1480nm) Power Loss
                                                                                                                 IR Laser
                                         Power After the Attachment    Power Before the Attachment
                                                                                                              Wavelength        1480nm
                              400
                                                                                                              Laser Power
                                                                                                              (max)             400mW
                              350
                                                                                                             Power at
                                                                                                            Diamond Tip         140mW
    Output Laser Power (mw)




                              300
                                                                                                              Photon energy       ~0.9 eV
                              250                                                                             Transitivity of Si-
                                                                                                              II                  80-90 %
                              200
                                                                                                               Absorbance in
                                                                                                            Si-II                 10.0 %
                              150
                                                                                                              Diamond tool
                              100
                                                                                                                                5-6 μm
                                                                                                              Diameter of tip
                                                                                                                                900-1200
                                                                                                              Thermal
                              50
                                                                                                              conductivity      W/m/K
                               0
                                                                                                                 Silicon
                                    0                  500                  1000                     1500
                                                                                                              Specific heat     0.7J/g/K
                                                                                                                                2.33 g/cm3
                                                       Laser Driving Current (mA)                             Density

                                                                                                                                        8
MSEC-2008 ASME Conference, Evanston, IL
IR Softens Metallic Silicon
       Indent depths at different laser power

                                   Fiber

                                                   Weights


                                                                            Scratch and stay test (load 25mN)




                                               Si Wafer




                                                                 Scratching Speed Test (Load 25mN)
                                           Speed1: 0.305 mm/sec; Speed 2: 0.002 mm/sec; Speed 3:.0002mm/sec

                                                                                                                9
MSEC-2008 ASME Conference, Evanston, IL
AFM Groove Depth Measurement




                                             10
MSEC-2008 ASME Conference, Evanston, IL
Thermal Imaging : Different Stages of
                     Heating
                     Stage :1




                                                11
MSEC-2008 ASME Conference, Evanston, IL
Thermal Imaging : Different Stages of
                     Heating
                     Stage :2




                                                12
MSEC-2008 ASME Conference, Evanston, IL
Thermal Imaging : Different Stages of
                     Heating
                     Stage :3




                                                13
MSEC-2008 ASME Conference, Evanston, IL
Thermal Imaging : Different Stages of
                     Heating
                     Stage :4




                                                14
MSEC-2008 ASME Conference, Evanston, IL
Thermal Imaging : Different Stages of
                     Heating
                     Stage :5




                                                15
MSEC-2008 ASME Conference, Evanston, IL
Thermal Imaging : Different Stages of
                     Heating
                     Stage :6




                                                16
MSEC-2008 ASME Conference, Evanston, IL
17
Estimation of Physical
              properties of Si-II and their use in
                          modeling
                                        Thermal
                                                       1. Analytical modeling
         Temperature                 Conductivity of
                                                          The thermo-physical properties are
             (K)                      metallic Si-II
                                                          taken at intermediate temperature.
                                        W/cm/K
                300                   0.0025
                                                       2. FEM formulation
                400                   0004
                                                           Thermo physical properties of si-I
                500                   0.0055
                                                              and Si-II are taken as function
                600                   0.0075
                700                   0.0125                  of Temperature
                800                   0.0165
                900                   0.025


         •MatLab is used for programming analytical model
         •COMSOL 3.4 is used for FEA


                                                                                            18
MSEC-2008 ASME Conference, Evanston, IL
Analytical Modeling
     1. Moving point heat source ( scratch test)
                                                                                               2       2       2
                                                                                           x       y       z
                                                                       t
                                                 2 q (1   r)               d                       4t
                                          T                                            e
                                                               3               3
                                                                   2               2
                                              Cp     4                 0




                                            :Thermal Diffusivity (cm2/s)
                                          r : Reflectivity
                                          Ρ : Density (g/cm3)
                                          k : Thermal Conductivity
                                                     W/cm/K



                                                                                                                   19
MSEC-2008 ASME Conference, Evanston, IL
Analytical Modeling….
                  2. Moving Plane Heat Source
                                                                                  t
                                                                          2                               2
                                                                      v                               u
                                                                 Xv           4a
                                          2 q (1   r )v                               d               2a
                                                                 2a
                             T                               e                                    e
                                                     3                                    3
                                                         2                                    2
                                     16 k                                     0




                                            :Thermal Diffusivity (cm2/s)
                                          r : Reflectivity
                                          Ρ : Density (g/cm3)
                                          k : Thermal Conductivity
                                                     W/cm/K




                                                                                                              20
MSEC-2008 ASME Conference, Evanston, IL
Analytical Modeling….
            3. Gaussian Beam profile Moving Plane
       with Laser as heating source (scratch test)
                                                                                                                                               2
                                                                                                              2
                                                                                                  x                               y
                                          I x, y              I o exp
         Gaussian Profile                                                                         rx                              ry


                                                                   Q1                         r
         Temperature                            T ( x, y, z )                                                 f ( u ) du
                                                                                  3
                                                                                          k
                                                                                      2

         Profile                                                                                      0



                                                                                                          2
                                                                                                  2

         Temperature                                               X              V           u                                   2                    2
                                                                                                                          Y                        Z
                                                       ex p                                                               2                            2
                                                                                          1
                                                                              2
                                                                                                                      u                            u
                                                                      u
         function                         f (u )                                                                                       1
                                                                                                                                           2
                                                                                          1
                                                                          2                                   2
                                                                      u                                   u

         Non-dimensional
         parameter                                                                                                                                                                     1
                                                                                                                                                                                           2
                                                                                                                                                                               2t
                                                                                                                                                               2
                                                   x                                                                          v                                        q
                                                                  y                               z                                                        r               u
                                                              Y                       Z
                                            X                                                                     V                                                Q               2
                                                                                                                                                                               r
                                                   r                                                                          r                                        r
                                                                  r                               r                                                        4




                                                                                                                                                                                               21
MSEC-2008 ASME Conference, Evanston, IL
3. Gaussian Beam profile Moving Plane…….
                                          Temperature Profile




                                                                22
MSEC-2008 ASME Conference, Evanston, IL
Finite Element Analysis




                                                       23
MSEC-2008 ASME Conference, Evanston, IL
Summary
     • Thermal images: the absorptivity of the Si-II is
       different than the Si-I and therefore the
       temperature rise occurs is due to HPPT
     • The temperature rise for the stationary point heat
       source is 778oC.
     • For the moving plane heat source T at 0.0002
       mm/sec, is 468oC,
     • The COMSOL result, for a stationary heat source
       temperature rise of 631oC. The COMSOL results
       are in good agreement with the previous estimated
       temperature

                                                        24
MSEC-2008 ASME Conference, Evanston, IL
Future Work
• Numerical Analysis of the Moving laser with
  varying laser power with varying absorption
  with the depth.
• Investigate the possibility of other
  wavelength.
• Machining using chemical etching
• Investigation of acoustic emission of the
  machining process

                                                25
References
     [1] Abdel-Aal, H. A., Y. Reyes, et al. (2006). quot;Extending electrical resistivity measurements in micro-scratching of silicon to
           determine thermal conductivity of the metallic phase Si-II.quot; Materials Characterization 57(4-5): 281-289.
     [2] Carslaw, H. S. and J. C. Jeager (1953). Conduction of Heat in Solids. Clarendon, UK, Oxford.
     [3] Dong, L. (2006). In-situ detection and heating of high pressure metallic phase of silicon during scratching. United
           States -- North Carolina, The University of North Carolina at Charlotte., PhD Dissertation, Mechanical Engineering
           Dept.
     [4] Hanfland, M., M. Alouani, et al. (1988). quot;Optical properties of metallic silicon.quot; Physical Review B 38(18): 12864.
     [5] Hou, Z. B. and R. Komanduri (2000). quot;General solutions for stationary/moving plane heat source problems in
           manufacturing and tribology.quot; International Journal of Heat and Mass Transfer 43(10): 1679-1698.
     [6] Komanduri, R. and Z. Hou (2000). quot;Thermal analysis of the arc welding process: Part I. General solutions.quot;
           Metallurgical and Materials Transactions B 31(6): 1353-1370.
     [7] Komanduri, R. and Z. B. Hou (2001). quot;Analysis of heat partition and temperature distribution in sliding systems.quot;
           Wear 251(1-12): 925-938.
     [8] Lide, D. R. (2003-2004). CRC Handbook of Chemistry and Physics, Student Edition, CRC Press.
     [9] Moody, J. E. and R. H. Hendel (1982). quot;Temperature profiles induced by a scanning cw laser beam.quot; Journal of Applied
           Physics 53(6): 4364-4371.
     [10] Trefilov, V.I., Milman, Y.V., “Sbornik Voprosyi Fiziki metallov i metallo-vedeniya”, Vol. 17, Izd. Akad. Nauk Ukr.SSR, 45
           (1963).
     [11] Palik, E.D., Handbook of Optical Constants of Solids. 1st ed, ed. E.D. Palik. 1997: Academic Press. 3224.Moody, J..
     [12] Engineering, E. & C. Complex Index of Refraction Look-up Utility. 2008 [cited 2008 June 15, 2008]; Available from:
           http://www.ee.byu.edu/photonics/opticalconstants.phtml.
     [13] Trefilove, V.I., Milman, Y. V., “Sbornik Voprosyi Fiziki Metallov I metallo-vedeniya”, Vol. 17,Izd. Akad. Nauk Ukr.
              SSR, 45 (1963).




                                                                                                                                26
MSEC-2008 ASME Conference, Evanston, IL
Thank you




                                                      27
MSEC-2008 ASME Conference, Evanston, IL

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Si Laser Micro Machining

  • 1. Estimation of Temperature Distribution in Silicon during Micro Laser Assisted Machining Presented by Kamlesh Suthar John Patten* Western Michigan University Manufacturing Engineering Department Kalamazoo, MI-49008, USA Lei Dong Hisham Abdel-Aal Condor USA, Inc. Department of General Engineering 8318 Pineville-Matthews Road, Suite 276 University of Wisconsin at Platteville Charlotte, NC-28226 Platteville, WI- 53818, USA
  • 2. Outline Objective Analytical Finite Element Experimental work Modeling Analysis • Tool • Point heat • Gaussian Profile Modification source heat source • Measurement of • Plane Heat laser power source • Characterization • Gaussian Beam Laser Heat • AFM Source • Thermal imaging Summary 2 MSEC-2008 ASME Conference, Evanston, IL
  • 3. Motivation • Semiconductor and ceramic materials are highly brittle and plastic deformation at room temperature is difficult and they prone to fracture during machining • Brittleness has detrimental effect on tool • Therefore, the challenge is to develop a cost effective machining process which can produce ultra fine surface finish 3 MSEC-2008 ASME Conference, Evanston, IL
  • 4. Objective • Silicon is highly brittle at room temperature and the hardness is the function of temperature • High Pressure Phase Transformation (HPPT) is one of the process mechanisms involved in ductile machining of semiconductors and ceramics. • Preferentially heat the HPPT material to increase ductility through thermal softening – Reduce tool wear – Minimize surface and subsurface damage. • Thermal Softening temperature for silicon is 600- 800 oC 4 MSEC-2008 ASME Conference, Evanston, IL
  • 5. Effect of Temperature on Hardness of Silicon (Trefilov,1963) 5
  • 6. Schematic of -LAM of Silicon 6 MSEC-2008 ASME Conference, Evanston, IL
  • 7. Diamond Tip Attachment 250 um 90 Conical Tip 5 μm radius Attachment was done at Digital Optical Company (Charlotte, NC) by Jay Matthews 7 MSEC-2008 ASME Conference, Evanston, IL
  • 8. Deliverable Power After Attachment of Diamond & Laser Parameter Laser (0~400mw,1480nm) Power Loss IR Laser Power After the Attachment Power Before the Attachment Wavelength 1480nm 400 Laser Power (max) 400mW 350 Power at Diamond Tip 140mW Output Laser Power (mw) 300 Photon energy ~0.9 eV 250 Transitivity of Si- II 80-90 % 200 Absorbance in Si-II 10.0 % 150 Diamond tool 100 5-6 μm Diameter of tip 900-1200 Thermal 50 conductivity W/m/K 0 Silicon 0 500 1000 1500 Specific heat 0.7J/g/K 2.33 g/cm3 Laser Driving Current (mA) Density 8 MSEC-2008 ASME Conference, Evanston, IL
  • 9. IR Softens Metallic Silicon Indent depths at different laser power Fiber Weights Scratch and stay test (load 25mN) Si Wafer Scratching Speed Test (Load 25mN) Speed1: 0.305 mm/sec; Speed 2: 0.002 mm/sec; Speed 3:.0002mm/sec 9 MSEC-2008 ASME Conference, Evanston, IL
  • 10. AFM Groove Depth Measurement 10 MSEC-2008 ASME Conference, Evanston, IL
  • 11. Thermal Imaging : Different Stages of Heating Stage :1 11 MSEC-2008 ASME Conference, Evanston, IL
  • 12. Thermal Imaging : Different Stages of Heating Stage :2 12 MSEC-2008 ASME Conference, Evanston, IL
  • 13. Thermal Imaging : Different Stages of Heating Stage :3 13 MSEC-2008 ASME Conference, Evanston, IL
  • 14. Thermal Imaging : Different Stages of Heating Stage :4 14 MSEC-2008 ASME Conference, Evanston, IL
  • 15. Thermal Imaging : Different Stages of Heating Stage :5 15 MSEC-2008 ASME Conference, Evanston, IL
  • 16. Thermal Imaging : Different Stages of Heating Stage :6 16 MSEC-2008 ASME Conference, Evanston, IL
  • 17. 17
  • 18. Estimation of Physical properties of Si-II and their use in modeling Thermal 1. Analytical modeling Temperature Conductivity of The thermo-physical properties are (K) metallic Si-II taken at intermediate temperature. W/cm/K 300 0.0025 2. FEM formulation 400 0004 Thermo physical properties of si-I 500 0.0055 and Si-II are taken as function 600 0.0075 700 0.0125 of Temperature 800 0.0165 900 0.025 •MatLab is used for programming analytical model •COMSOL 3.4 is used for FEA 18 MSEC-2008 ASME Conference, Evanston, IL
  • 19. Analytical Modeling 1. Moving point heat source ( scratch test) 2 2 2 x y z t 2 q (1 r) d 4t T e 3 3 2 2 Cp 4 0 :Thermal Diffusivity (cm2/s) r : Reflectivity Ρ : Density (g/cm3) k : Thermal Conductivity W/cm/K 19 MSEC-2008 ASME Conference, Evanston, IL
  • 20. Analytical Modeling…. 2. Moving Plane Heat Source t 2 2 v u Xv 4a 2 q (1 r )v d 2a 2a T e e 3 3 2 2 16 k 0 :Thermal Diffusivity (cm2/s) r : Reflectivity Ρ : Density (g/cm3) k : Thermal Conductivity W/cm/K 20 MSEC-2008 ASME Conference, Evanston, IL
  • 21. Analytical Modeling…. 3. Gaussian Beam profile Moving Plane with Laser as heating source (scratch test) 2 2 x y I x, y I o exp Gaussian Profile rx ry Q1 r Temperature T ( x, y, z ) f ( u ) du 3 k 2 Profile 0 2 2 Temperature X V u 2 2 Y Z ex p 2 2 1 2 u u u function f (u ) 1 2 1 2 2 u u Non-dimensional parameter 1 2 2t 2 x v q y z r u Y Z X V Q 2 r r r r r r 4 21 MSEC-2008 ASME Conference, Evanston, IL
  • 22. 3. Gaussian Beam profile Moving Plane……. Temperature Profile 22 MSEC-2008 ASME Conference, Evanston, IL
  • 23. Finite Element Analysis 23 MSEC-2008 ASME Conference, Evanston, IL
  • 24. Summary • Thermal images: the absorptivity of the Si-II is different than the Si-I and therefore the temperature rise occurs is due to HPPT • The temperature rise for the stationary point heat source is 778oC. • For the moving plane heat source T at 0.0002 mm/sec, is 468oC, • The COMSOL result, for a stationary heat source temperature rise of 631oC. The COMSOL results are in good agreement with the previous estimated temperature 24 MSEC-2008 ASME Conference, Evanston, IL
  • 25. Future Work • Numerical Analysis of the Moving laser with varying laser power with varying absorption with the depth. • Investigate the possibility of other wavelength. • Machining using chemical etching • Investigation of acoustic emission of the machining process 25
  • 26. References [1] Abdel-Aal, H. A., Y. Reyes, et al. (2006). quot;Extending electrical resistivity measurements in micro-scratching of silicon to determine thermal conductivity of the metallic phase Si-II.quot; Materials Characterization 57(4-5): 281-289. [2] Carslaw, H. S. and J. C. Jeager (1953). Conduction of Heat in Solids. Clarendon, UK, Oxford. [3] Dong, L. (2006). In-situ detection and heating of high pressure metallic phase of silicon during scratching. United States -- North Carolina, The University of North Carolina at Charlotte., PhD Dissertation, Mechanical Engineering Dept. [4] Hanfland, M., M. Alouani, et al. (1988). quot;Optical properties of metallic silicon.quot; Physical Review B 38(18): 12864. [5] Hou, Z. B. and R. Komanduri (2000). quot;General solutions for stationary/moving plane heat source problems in manufacturing and tribology.quot; International Journal of Heat and Mass Transfer 43(10): 1679-1698. [6] Komanduri, R. and Z. Hou (2000). quot;Thermal analysis of the arc welding process: Part I. General solutions.quot; Metallurgical and Materials Transactions B 31(6): 1353-1370. [7] Komanduri, R. and Z. B. Hou (2001). quot;Analysis of heat partition and temperature distribution in sliding systems.quot; Wear 251(1-12): 925-938. [8] Lide, D. R. (2003-2004). CRC Handbook of Chemistry and Physics, Student Edition, CRC Press. [9] Moody, J. E. and R. H. Hendel (1982). quot;Temperature profiles induced by a scanning cw laser beam.quot; Journal of Applied Physics 53(6): 4364-4371. [10] Trefilov, V.I., Milman, Y.V., “Sbornik Voprosyi Fiziki metallov i metallo-vedeniya”, Vol. 17, Izd. Akad. Nauk Ukr.SSR, 45 (1963). [11] Palik, E.D., Handbook of Optical Constants of Solids. 1st ed, ed. E.D. Palik. 1997: Academic Press. 3224.Moody, J.. [12] Engineering, E. & C. Complex Index of Refraction Look-up Utility. 2008 [cited 2008 June 15, 2008]; Available from: http://www.ee.byu.edu/photonics/opticalconstants.phtml. [13] Trefilove, V.I., Milman, Y. V., “Sbornik Voprosyi Fiziki Metallov I metallo-vedeniya”, Vol. 17,Izd. Akad. Nauk Ukr. SSR, 45 (1963). 26 MSEC-2008 ASME Conference, Evanston, IL
  • 27. Thank you 27 MSEC-2008 ASME Conference, Evanston, IL