Routine impurity analysis with UPLC/MS and UPC2/MS
Abu @50 musrl power pt presentation
1. ABU @ 50
FACILITIES IN THE MULTI-USER
SCIENCE RESEARCH LABORATORY
(MUSRL) AHMADU BELLO
UNIVERSITY, ZARIA
PRESENTED BY:
SILAS EKWURIBE (HND,MNIST,ICCON)
(LABORATORY MANAGER, MUSRL)
2.
3. LOCATION OF MUSRL
MULTI-USER SCIENCE RESEARCH
LABORATORY (MUSRL) IS
SITUATED AT THE DEPARTMENT
OF CHEMISTRY. AHMADU BELLO
UNIVERSITY ZARIA.
4. • VISION: To promote inter-disciplinary
research using state of the art equipment in
generating qualitative and reliable results
comparable with that of any world class
laboratory.
• MISSION: To produce a new breed of highly
skilled scientists and establish standards which
do not only serve as a template for other
Laboratories in Nigeria but equally meet
International Standards.
5. INFRASTRUCTURES OF MUSRL
• THE MULTI-USER SCIENCE RESEARCH LABORATORY (MUSRL), AHMADU
BELLO UNIVERSITY CONT’D
• THE LABORATORY IS A STORY BUILDING DESIGNED TO ACCOMMODATE
THE FOLLOWING:
• GROUND FLOOR:
• ADMINISTRATIVE OFFICE
• SECRETARY’S OFFICE
• LABORATORY STORE
• WORK BENCH ACCOMODATING EQUIPMENT
• CENTRAL AREA SUITABLE FOR WORKSHOPS, GROUP DISCUSSIONS AND
SEMINAR PRESENTATIONS
• FIRST FLOOR:
• SIX ROOMS TO ACCOMMODATE SPECIAL EQUIPMENTS
• CENTRAL AREA SUITABLE FOR WORKSHOPS, GROUP DISCUSSIONS AND
SEMENAR PRESENTATIONS
6. INFRASTRUCTURES OF MUSRL CONT’D
ADMINISTRATIVE OFFICE SECRETARY’S OFFICE
LABORATORY WORK SPACE AND SOME EQUIPMENTS.THE CENTRAL
SPACE IS AVAILABLE FOR SEMINARS AND WORKSHOPS
7. INFRASTRUCTURES OF MUSRL CONT’D
DUST CONTROL
THE WINDOWS AND DOORS OF THE
MUSRL ARE DESIGNED TO BE DUST
TIGHT.
BAIONAIRE PARTICULATE AIR FILTER
Dust is a notable enemy to the
production of accurate laboratory
results therefore each of our eight
(8) instrument rooms is equipped with
EQUIPMENT ROOMS OFFICES
a particulate air filter. All vents and
AND THE CENTRAL SPACE FOR
windows are designed to be dust-
WORKSHOPS FULLY
tight.
8. INFRASTRUCTURES OF MUSRL CONT’D
POWER SUPPLY
100KVA & 5KVA GENERATORS ON THE STANDBY INCASE OF
POWER FAILURE
9. INFRASTRUCTURES OF MUSRL CONT’D
GAS CYLINDER CAGE
FOR SAFETY REASONS, ALL TOXIC, FLAMABLE, IRRITANT AND POISONOUS GAS CYLINDERS ARE HOUSED IN A
CAGE OUTSIDE THE LABORATORY AND PIPED TO THE POINTS WHERE THEY ARE NEEDED IN THE ROOMS
10. INFRASTRUCTURES OF MUSRL CONT’D
SAFETY GADJETS
PREMIER SX ALARM CONTROL Fire extinguishers and fire
SYSTEM & SMOKE DETECTOR. blankets available at strategic
Installed to detect any fire locations in the laboratory, incase
outbreak of fire outbreak
11. EQUIPMENT IN THE MULTI-USER SCIENCE RESEARCH
LABORATORY (MUSRL)
SPECIAL FEATURES: equipped with graphite furnace, vapor generator assembly( VGA)
auto sampler & assorted multi-element lamps.
LAMPS & STANDARDS ARE AVAILABLE FOR THE FOLL0WING ELEMENTAL ANALYSIS:
aluminum, antimony, arsenic, barium, beryllium, bismuth ,boron, chromium, cadmium,
calcium, cobalt, copper, gold, iron, lead, lithium, magnesium, mercury, molybdenum,
nickel, palladium, platinum, potassium, silicon, silver, selenium, sodium, titanium,
tungsten, tin, vanadium, zinc.
12. DIFFERENTIAL SCANNING CALORIMETER (DSC)
One of the latest addition to the Lab is the DSC. It is used to
determine the temperature and heat of transformation in both liquid
and solid materials: measures physical properties like compatibility,
purity, crystallization, heat capacity and evaporation. It also assesses
stability and the kinetic profile of materials and is useful for food ,
pharmaceutical and material sciences.
13. EQUIPMENT IN THE MULTI-USER SCIENCE RESEARCH
LABORATORY (MUSRL) CONT,D
Oxford XRF (X-SUPREME)
SUPPORTING EQUIPMENT FOR THE XRF
Analysis both solid and liquid samples,
Our X-Ray fluorescence is employed in
Investigations that involve bulk chemical
analyses of major and trace elements like Si, Ti, Retsch RS200 milling machine, jaw
Al, Fe, Mn, Mg, Ca, Na, K, P Ba, Ce, Co, Cr, Cu, Ga, crusher, MM400, Specac press
La, Nb, Ni, Rb, Sc, Sr, Rh, U, V, Y, Zr, Zn) in rock machine for solid sample
and sediment - preparation, for the XRF
14. AMINO ACID ANALYSZER (SYCAM)
The automated Amino Acid Analyzer is
employed in;
the analysis of nutritive values of food stuffs,
agricultural products
and Physiological Fluids in medical research.
15. THE CHNS-O ELEMENTAL ANALYSER
This equipment is used for the
determination of the
composition of carbon,
hydrogen, nitrogen, and
oxygen components of organic
samples.
AREA OF APPLICATION:
petrochemical industry
geological industry
agricultural industry
Pure Organic Samples
Synthetic Mixtures
Organometallic
Plastic & Polymer Rubber
Coal & Coke.
Soils and Sediments
Plants; Compost & Leaves
Fertilizers industry
Animal Feed
16. OLYMPUS BX 41 RESEARCH MICROSCOPE
This microscope allows for clearer, brighter, beautifully
contrasted images. It also has multiple condensers to allow for
an array of contrast techniques, including bright field, dark
field, differential interference contrast (DIC), polarization, and
phase contrast. It has a wide-range of applications and is
especially suited for clinical research.
17. EQUIPMENT IN THE MULTI-USER SCIENCE RESEARCH LABORATORY
(MUSRL) CONT,D
DEIONIZED WATER KIT
Millipore water purification System for ultra pure Deionized
water
18. EQUIPMENT IN THE MULTI-USER SCIENCE
RESEARCH LABORATORY (MUSRL) CONT,D
Weighing; a fundamental step to accuracy and precision
is achieved with our SARTORIUS GEM & GOLD EXTEND SERIES ANALYTICAL
BALANCE
20. EQUIPMENT IN THE MULTI-USER SCIENCE RESEARCH LABORATORY
(MUSRL) CONT,D
HACH CEL/890 WATER
TESTING KIT
Our CEL/890 is used to perform Tests on High pressure boiler water,
Demineralized
Water, Drinking water, Waste water, surface Water Industrial process
water, Concentrated acids & dyes We determine DO, BOD, COD, pH,
turbidity, salinity, suspended solids and other physicochemical
parameters In water; viz. chlorine (DPD method), Hardness, iron,
manganese ,tannin and lignin, Nitrogen, organic carbon, silica,
21. OTHER EQUIPMENT IN THE MULTI-USER SCIENCE RESEARCH
LABORATORY (ETF, ABU)
JENWAY 3505 PH METER
SANYO INCUBATOR
JENWAY UV-SPECTROPHOTOMETERS
FISHER HIGH SPEED CENTRIFUGE
22. EQUIPMENT YET TO BE INSTALLED IN THE MULTI-USER SCIENCE
RESEARCH LABORATORY
VARIAN ANALYTICAL HPLC
BUCHI SPRAY DRYER
LABOMED UV-SPECTROPHOTOMETER
HELIOS UV-SPECTROPHOTOMETER
CLARIUS 600 GC-MS
VIRTIS FREEZE DRYER
Is 10 FTIR
23. EQUIPMENT IN THE MULTI-USER SCIENCE
RESEARCH LABORATORY (MUSRL) CONT,D
ASYS MICROPLATE READER
24. STATISTICS OF EQUIPMENT & EQUIPMENT USAGE .
AUG. 2010 – MARCH 2012
Atomic Absorption spectrophotometer,
Hach Advance portable Laboratory kit, pH Meters, Bench services etc
No OF USERS NO OF SAMPLES
MONTH YEAR
AUGUST 2011 02 203
SEPTEMBER 2011 11 60
OCTOBER 2011 10 165
NOVEMBER 2011 14 1588
DECEMBER 2011 10 350
JANUARY 2012 02 7
FEBUARY 2012 13 58
MARCH 2012 14 545
SUB TOTAL 76 2976
25. STATISTICS OF EQUIPMENT & EQUIPMENT USAGE .
AUG. 2010 – SEPTEMBER 2012 CONT’D
Atomic Absorption spectrophotometer,
Hach Advance portable Laboratory kit, pH Meters, Bench services etc
No OF USERS NO OF SAMPLES
MONTH YEAR
APRIL 2012 05 115
MAY 2012 18 360
JUNE 2012 21 241
JULY 2012 33 294
AUGUST 2012 27 350
SEPTEMBER 2012 10 129
SUB TOTAL 1489
26. USERS STATISTICS (AAS):
OTHER INSTITUTIONS
MONTH UNIVERSI UNIVERSI UNIV. BAYERO NUHU U/DAFODI
TY OF JOS TY OF AGRIC. UNIVERSI BAMALLI O
MAIDUGR MAKURDI TY
I
AUG. - 1 - - - -
SEPT 2 1 1 - - -
OCT. - 2 2 - - -
NOV. - - - 1 -
DEC. - 1 - 2 -
JAN. - - - - 1 -
FEB. - - - - - 1
MAR. - - - - - -
27. USERS STATISTICS: AHMADU BELLO UNIVERSITY
MONTH CIVIL CHEM BIOCHE AGRIC MIRO CHE BIO PHAR BIOTEC
ENG.A ENG. M. ABU C/PLE BIO M. SC. M. H
BU ABU X. ABU ABU ABU ABU
AUG. 2011 - - 1 1 - 6 - - -
SEPT. 2011 - - 5 - - 2 - - -
OCT. 2011 1 - 3 - 1 2 - - -
NOV. 2011 - - 2 3 - 4 2 - -
DEC. 2011 - - - - 1 5 - - -
JAN. 2012 - - - - - 1 - - -
FEB. 2012 - - 2 - 5 1 1 -
MAR. 2012 - 3 1 1 6 - 1