1. 1
Powder Piloting Service
Material solutions, from powder to product.
VTT Technical Research Centre of Finland Ltd
Service for Additive Manufacturing (AM)
www.vtt.fi/powder
2. 2
Service for introducing new material
compositions to SLM from materials to
performance validated product.
Utilization of AM technologies such as
Selective Laser Melting increases rapidly
Number of commercially available AM
customized powders is limited and pricing
of is high
Additive Manufacturing (AM)
www.vtt.fi/powder
3. 305/12/2017 3
Selection of material composition meeting demands of component
operation conditions
Evaluation of material suitability to SLM process (thermodynamics,
phase structures)
2
1
3
4
5
Material selection
and design
Powder processing &
modification to SLM
Processing
parameters for SLM
Processing of
test components
Design and
manufacturing of
real component
Development steps from powder to product:
Additive Manufacturing (AM)
Is there powder commercially available with needed properties?
modification of power properties to meet demands of SLM
production of powder with desired specs
Processing and modification of powders to meet process demands
Design of experiment (DoE) for process parameter mapping
DoE based processing parameter optimization
Heat treatments, HIP, grinding, machining, polishing
Specimens for lab material testing e.g. tensile test specimens in
different orientations
Design and optimization of component for SLM process and for
operation conditions
Manufacturing and post treating of component
Component performance testing (lab and/or field testing)
www.vtt.fi/powder
4. 405/12/2017 4
Development steps from powder to product:
Additive Manufacturing (AM)
Does processing parameters lead to
desired properties?
GATE2.
Does material properties meet
demands of component?
GATE3.
Does powder fill demands
of SLM process?
GATE1.
www.vtt.fi/powder
2
1
3
4
5
Material selection
and design
Processing
parameters for SLM
Processing of
test components
Design and
manufacturing of
real component
Powder processing &
modification to SLM
5. 505/12/2017 5
Demands and restrictions from operation conditions
Strength, corrosion etc.
Demands and restrictions of SLM process
Thermodynamics, prediction of phase structures, need for preheat,…
Powder properties, flowability, packing density, particle size distribution
STEP 1. Material selection & design
Additive Manufacturing (AM) www.vtt.fi/powder
6. 605/12/2017 6
Can be done by “light” more traditional way or by ICME approach.
STEP 1. Material selection & design
Additive Manufacturing (AM) www.vtt.fi/powder
7. 705/12/2017 7
Is there powder commercially available with needed properties?
If yes, modification of power properties to meet demands of SLM
If no, production of powder with desired specs
Possible technologies
Atomization, milling, air classification, plasma spheroidization,…
Characterization of properties
STEP 2. Powder processing & modification
Additive Manufacturing (AM) www.vtt.fi/powder
8. 805/12/2017 8
400
600
800
1000
1200
100 150 200 250 300
Scanningspeed(mm/s)
Power (W)
VED 50 VED 100
Experimental designs
Using D-optimal design
of experiments.
Printing samples and
measuring density using
image analysis.
Fitting a numerical
model and calaculating
the optimal parameters.
90
100
110
120
130
140
150
400 900
Hatchwidth(µm)
Scanning speed (mm/s)
VED 50 VED 100
Hatchwidth(µm)Scanningspeed(mm/s)
Scanning speed (mm/s)
Power (W)
STEP 3: Processing parameters for SLM
Additive Manufacturing (AM) www.vtt.fi/powder
9. 905/12/2017 9
Post treatment
Heat treatments according to targeted
structural properties
Densification and homogenization by
hot isostatic pressing if necessary
Surface grinding & polishing
Desired performance testing
Heat treatment Procedure Hardness
Stress relief anneal Held at 650°C for 2h 45 HRC
Hardening and tempering Held at 1030°C for 30min + quench in oil
Tempered at 400°C for 2+2h
55 HRC
Conventionally manufactured
(Reference)
Held at 1025°C for 30min + quench in air
Tempered at 550°C for 2+2h
52 HRC
0
200
400
600
800
1000
1200
1400
1600
1800
2000
Stress(MPa)
Initial Optimized Reference
Ultimate tensile strength (Horizontal)
As built
Stress relief
annealed
Hardened
and
tempered
STEP 4: Processing of test components
Additive Manufacturing (AM) www.vtt.fi/powder
10. 1005/12/2017 10
Co-creation with VTT experts
Re-design for AM, topological optimization
Real, printed case component
Component performance testing
Cost estimation of manufacturing of case component
Component
selection
Redesign
3D printing
Cost estimation
STEP 5: Design and manufacturing of real
component
Additive Manufacturing (AM) www.vtt.fi/powder
11. 111105/12/2017
Material H13 tool steel
Optimized mass: 489 g (compared to original
mass 1.446 kg) 66% reduction
No drilling no pluging no leaking!
Better fluid flow due to optimized fluid channels
Will be still further optimized
Final version will be tested in operative conditions
Case 3D printed optimized hydraulic
valve block
Additive Manufacturing (AM) www.vtt.fi/powder