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Delamination of a Strong Thin Film From a Ductile Substrate
                                 During Indentation Loading and Unloading
                                                                                Adnan Abdul-Baqi & Erik van der Giessen
                                                                                                                          Koiter Institute Delft


Introduction                                                                                                                             The cohesive surface model

Indentation loading and unloading of a strong elastic                                                                                    In the description of the interface as a cohesive surface, a small dis-
film on a ductile substrate is modeled. The film is con-                                                                                   placement jump ∆ between the film and substrate is allowed, with nor-
sidered to be elastic, the substrate is elastic perfectly-                                                                               mal and tangential components ∆ n and ∆ t respectively. The
plastic and the indenter is spherical and rigid (Fig. 1).                                                                                corresponding tractions we adopt in this study are those used by Xu and
The interface is modeled by means of a cohesive surface.                                                                                 Needleman [1]. Figure 2 shows these tractions in their uncoupled form.

                ˙
                h                                                                                                1.5                                                                                          3
                                                                                                                                             ∆t = 0
                                                                                                                  1                                                                                           2                                                                       ∆n = 0
                                 R                                                                               0.5
                                                                                                                                                                                                              1
                     a                                                                                            0




                                                                                                                                                                                                    t max
                                                                                                          max




                                                                                                                                           increasing ∆ t                                                     0




                                                                                                                                                                                              T /τ
                                                                                                                −0.5
                                                                                                        T /σ




h
                                                                                                          n




                                                  coating           t                                            −1                                                                                         −1
                                                                                                                                                                                                                                                                     increasing ∆ n
                                                                                                                −1.5
                                                  interface                                                                                                               (a)                               −2
                                                                                                                                                                                                                                                                                      (b)
                                                                                                                 −2

                                                  substrate                                                     −2.5
                                                                                                                  −1          0    1         2             3          4     5          6
                                                                                                                                                                                                            −3
                                                                                                                                                                                                             −3             −2           −1               0                 1          2          3
                                                                                                                                                   ∆n/δn                                                                                                 ∆t/δt

           Figure 1. Geometry.                                                                          Figure 2. (a) Normal traction versus normal separation. (b) Tangential traction versus tangential separation.



Results
         0.00                                                                   σe/σy              0.00                                                                         σyy/σmax                     2
                                                                                                                                                                                                                      0.5
                                                                                                                                                                                                                                                                φ (J/m2)
                                                                                        1.40
                                                                                                                                                                                      1.0                                                                        n
                                                                                        1.26
                                                                                                                                                                                                                      0.4                            a
                                                                                        1.11                                                                                          0.8                 1.75                                                   a 150
         0.02                                                                           0.97       0.01                                                                               0.5                             0.3                            b           b 200
                                                                                        0.82
                                                                                                                                                                                      0.3                                                                        c 400
                                                                                        0.68                                                                                                                1.5       0.2
                                                                                        0.53                                                                                          0.1                                                c                       d 600
                                                                                        0.39                                                                                          -0.1                            0.1                                        e >> 600
         0.04                                                                           0.24       0.02                                                                                                   1.25                 d                e
                                                                                                                                                                                      -0.4                             0
                                                                                               z (mm)




                                                                                        0.10                                                                                                                            1      1.15 1.3 1.45 1.6 1.75
z (mm)




                                                                                                                                                                                      -0.6
                                                                                                                                                                                              F/(πR σy)
                                                                                                                                                                                              2




                                                                                                                                                                                                             1

         0.06                                                                                      0.03
                                                                                                                                                                                                          0.75



                                                                                                                                                                                                            0.5
         0.08                                                                                      0.04

                                                                                 (a)                                                                                            (b)                       0.25


         0.10                                                                                      0.05
            0.00          0.02             0.04            0.06    0.08     0.10                      0.00             0.01       0.02            0.03         0.04       0.05                               0
                                                                                                                                                                                                                  0     0.25       0.5        0.75         1         1.25       1.5        1.75   2
                                                  r (mm)                                                                                 r (mm)                                                                                                           h/t


Figure 3. (a) Contour plot of the Von Mises effective stress at the maximum indentation depth
                                                                                                                                                                                             Figure 4. Load versus displacement curves for dif-
( h max = 2t ), φ n = 150 ( J ⁄ m 2 ). Arrows show the shear direction, line shows the location of the tan-
                                                                                                                                                                                             ferent values of interfacial energies. Curve (e) repre-
gentially delaminated area. (b) Contour plot of the vertical stress component at the end of the unloading
                                                                                                                                                                                             sents the case of a perfect interface.
stage ( F = 0 ), φ n = 500 ( J ⁄ m 2 ).



                1
                                                                                                                         Conclusions
           0.8

                                                                                                                         1. For relatively weak interfaces, delamination occurs in the loading stage. It is
           0.6            E                                                                                              imprinted on the load vs displacement curve by a ‘kink’.
E/Emax




                           el
                          E
                           pl
                          E
                            int
           0.4
                          ∫ F dh                                                                                         2. Normal delamination occurs during the unloading stage, where a circular part
                          E + E +E
                            el   pl int

           0.2
                                                                                                                         of the coating is lifted off from the substrate. It is imprinted on the load vs dis-
                                                                                                                         placement curve by a ‘hump’.
                0
                 0                   0.5                      1           1.5                      2
                                                             h/t

Figure 5. Evolution of elastic, plastic, interfacial and
applied work during the loading and unloading process.                                                                   [1] X.-P. Xu, A. Needleman, Model. Simul. Mater. Sci. Eng. 1 (1993) 111.

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Delamination of thin strong film - poster

  • 1. Delamination of a Strong Thin Film From a Ductile Substrate During Indentation Loading and Unloading Adnan Abdul-Baqi & Erik van der Giessen Koiter Institute Delft Introduction The cohesive surface model Indentation loading and unloading of a strong elastic In the description of the interface as a cohesive surface, a small dis- film on a ductile substrate is modeled. The film is con- placement jump ∆ between the film and substrate is allowed, with nor- sidered to be elastic, the substrate is elastic perfectly- mal and tangential components ∆ n and ∆ t respectively. The plastic and the indenter is spherical and rigid (Fig. 1). corresponding tractions we adopt in this study are those used by Xu and The interface is modeled by means of a cohesive surface. Needleman [1]. Figure 2 shows these tractions in their uncoupled form. ˙ h 1.5 3 ∆t = 0 1 2 ∆n = 0 R 0.5 1 a 0 t max max increasing ∆ t 0 T /τ −0.5 T /σ h n coating t −1 −1 increasing ∆ n −1.5 interface (a) −2 (b) −2 substrate −2.5 −1 0 1 2 3 4 5 6 −3 −3 −2 −1 0 1 2 3 ∆n/δn ∆t/δt Figure 1. Geometry. Figure 2. (a) Normal traction versus normal separation. (b) Tangential traction versus tangential separation. Results 0.00 σe/σy 0.00 σyy/σmax 2 0.5 φ (J/m2) 1.40 1.0 n 1.26 0.4 a 1.11 0.8 1.75 a 150 0.02 0.97 0.01 0.5 0.3 b b 200 0.82 0.3 c 400 0.68 1.5 0.2 0.53 0.1 c d 600 0.39 -0.1 0.1 e >> 600 0.04 0.24 0.02 1.25 d e -0.4 0 z (mm) 0.10 1 1.15 1.3 1.45 1.6 1.75 z (mm) -0.6 F/(πR σy) 2 1 0.06 0.03 0.75 0.5 0.08 0.04 (a) (b) 0.25 0.10 0.05 0.00 0.02 0.04 0.06 0.08 0.10 0.00 0.01 0.02 0.03 0.04 0.05 0 0 0.25 0.5 0.75 1 1.25 1.5 1.75 2 r (mm) r (mm) h/t Figure 3. (a) Contour plot of the Von Mises effective stress at the maximum indentation depth Figure 4. Load versus displacement curves for dif- ( h max = 2t ), φ n = 150 ( J ⁄ m 2 ). Arrows show the shear direction, line shows the location of the tan- ferent values of interfacial energies. Curve (e) repre- gentially delaminated area. (b) Contour plot of the vertical stress component at the end of the unloading sents the case of a perfect interface. stage ( F = 0 ), φ n = 500 ( J ⁄ m 2 ). 1 Conclusions 0.8 1. For relatively weak interfaces, delamination occurs in the loading stage. It is 0.6 E imprinted on the load vs displacement curve by a ‘kink’. E/Emax el E pl E int 0.4 ∫ F dh 2. Normal delamination occurs during the unloading stage, where a circular part E + E +E el pl int 0.2 of the coating is lifted off from the substrate. It is imprinted on the load vs dis- placement curve by a ‘hump’. 0 0 0.5 1 1.5 2 h/t Figure 5. Evolution of elastic, plastic, interfacial and applied work during the loading and unloading process. [1] X.-P. Xu, A. Needleman, Model. Simul. Mater. Sci. Eng. 1 (1993) 111.