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IMPLEMENTATION OF
HAZARD ANALYSIS CRITICAL
 CONTROL POINT (HACCP)
SYSTEM TO THE ALCOHOLIC
   BEVERAGE INDUSTRY

                 Submitted by:

                 Abhishek Rana

                 Amber Awasthi

                 Ankita Pathania

                 Charul Sharma

                 Deepak Dhar

                 Devansh Jaiswal
INTRODUCTION

• Real target- minimization of unacceptable unsafe
  products
• Prior to initiating HACCP system, company must
  endeavor to put together HACCP plan :
 a) identify HACCP resources & assemble team
 b) describe food & its distribution method
 c) state clearly intended use & consumers
 d) develop a process flow diagram
 e) verify validity of this diagram in practice (operation)
• 2 most important stages- Fermentation & bottling
HACCP Team


Names of          Titles/responsibilities   Educational     Experience or training
members                                     qualification
Abhishek Rana     Clean up/sanitation       B. Tech (FST)             _

Amber Awasthi     Outside Expert            B. Tech (FST)             _

Ankita Pathania   Laboratory, Quality       B. Tech (FST)             _
                  Assurance
Charul Sharma     Plant Manager             B. Tech (FST)             _

Deepak Dhar       Production                B. Tech (FST)             _

Devansh Jaswal    Engineer                  B. Tech (FST)             _
Product Description
NAME OF PRODUCT               RED WINE

FOOD SAFETY CHARACTERISTICS   pH : 3.3-3.5
                              Alcoholic content : 11-15%
PACKAGING USED                Glass bottles sealed with cork with final
                              packaging of silver & gold paper ; bag in
                              boxes
LABELLING REQUIREMENTS        Alcohol content, sulphite declaration &
                              health warning statement
STORAGE & DISTRIBUTION        Store in dark, moderately humid place at
                              130C
INTENDED CONSUMERS            Adults

INTENDED USE                  Ready to drink, as an ingredient

SHELF LIFE                    Bottled : 2-3 years
                              Opened (refrigerator) : 1-2 weeks
INTENDED USE


  Intended use      • Retail, ingredient, institutional
Intended & likely
   consumers        • Adults, elderly

Distribution area   • Nationwide

Consumer of food    • Adults (70%), elderly(20%)

  Distribution      • Preferably refrigerated (130C)
RED WINE
• Red wine is made from dark-coloured
  (black) grape varieties
• Actual colour range- intense violet
  (young wines), brick red (mature wines)
  & brown (older red wines)
• Juice from most black grapes is
  greenish-white; red colour comes from
  anthocyanins present in the skin of the
  grape
• Red-wine production process involves
  extraction of colour & flavour
  components from grape skin.
Plant layout
PROMINENT HAZARDS IDENTIFIED

                  • Fruit with rotten parts
   PHYSICAL       • Bottle condition
                  • Cork sizing



                  • Pesticide residues
                  • Heavy metals
   CHEMICAL       • Residues of ethylene glycol & detergents
                  • Methanol content
                  • Ethyl carbamate formation




                  • Microbial contamination of culture
                  • Water microbiological quality
MICROBIOLOGICAL   • Presence of yeasts & LAB
                  • Cork microflora
CCP-1 (Harvesting)

• Grape harvesting is CCP comprising both physical & chemical hazards
• Physically, grapes should be sound without rotten parts, otherwise oxidative &
  microbial contamination can rapidly develop
• Harvesting should be conducted with greatest possible care & efficient disease
  management system should be applied
• Pesticides should be handled with care as they constitute chemical hazards.
• At time of harvest, the grapes must have also reached correct maturity when Brix
  & Total Acidity levels indicate maturity of wine
• Pesticide & fungicide residues on surface of berries constitute chemical hazards
• Rapid & simple gas chromatography- method for determination
• Maximum residue limits for pesticides (grapes & wines)- Codex Alimentarius (45)
• Bulk bins used for grapes transportation, should be effectively decontaminated
  to avoid any microbial infection
CCP-2 (Alcoholic Fermentation)

• carried out by strains of Saccharomyces cerevisiae
  - grows at low pH values typical for grape must (pH
  3.2–4)
• chemical hazards : heavy metals presence (As<0.2,
  Cd<0.01, Cu<1, Pb<0.3 mg/L), methanol content
  (300 mg/L ), ethyl carbamate content, pesticide
  residues (as mentioned in the Codex Alimentarius)
  & residues of detergents (absence) & ethylene
  glycol (absence)
• desirable temperature varies within the range of
  25–28◦C
CCP-3 (Must)
• Possible contamination of must
  with killer yeasts result in stuck
  fermentation
• Attention should be paid to
  added amount of                SO2
  i.e.175mg/L in order to inhibit
CCP-4 (Maturation)

• Maturation step often lasts 6–24 months & takes place in oak barrels
• During maturation a range of physical & chemical interactions occurs
  among barrel, surrounding atmosphere & maturing wine, leading to
  transformation of flavor and composition of wine
• Oak barrel should be fault-free & undergone decontamination treatment
• Wood must be free of pronounced or undesirable odors, which could
  taint the wine
• White wines are matured in oak for shorter periods than red wines & in
  conditioned barrels to release less extractable (tannins)
• Another CCP- inhibition of O2 penetration through wood or during
  racking & sampling of wine
• Extensive penetration can cause various sensory changes (oxidized odor,
  browning, loss of color in red wines, activation of spoilage bacteria &
  yeasts, development of ferric casse & precipitation of tannins)
CCP-5 (Stabilization)
• Reason for stabilization- production of permanently clear &
  flavor fault-free wine
• Procedure
  a) tartrate stabilization by chilling wine to near its freezing point
  & filtering or centrifuging to remove crystals
 b) protein stabilization with absorption, denaturation or
  neutralization by fining agents (bentonite)
 c) polysaccharide removal with pectinases that hydrolyze
  polymer, disturbing its protective colloidal action & filter
  plugging properties
 d) metal casse (Fe, Cu) stabilization
• Ferric casse is controlled by addition of agents (bentonites,
  proteins) controlling flocculation of insoluble ferric complexes
• Wines with Cu content greater than 0.5 mg/L are particularly
  susceptible to Cu casse formation
CCP-6 (Bottling)
• Wine is bottled in glass bottles sealed with cork which must pass a
  decontaminating step & an inspection control to assure absence of any
  defects & stability of product until its consumption
• Cork should be correctly sized, 6–7 mm bigger than inner neck diameter,
  to avoid any possible leaks
• Hazards include : cork microflora, residues of heavy metals, SO2,
  pesticides & detergents & absence of cracks, scratches & rifts in lute
• CL for cork is absence of LAB & yeast, which can be assured with
  microbiological analysis
• For long storage of wine longer & denser corks are preferred
• Headspace O2 might affect product quality by causing disease of “bottle”
• CL for SO2 – 175mg/L , for As < 0.2 mg/L, Cd < 0.01 mg/L, Cu < 1 mg/L, Pb
  < 0.3 mg/L
CCP-7 (Storage)

• Shipping & storage of wines at elevated temperatures can
  initiate rapid changes in color & flavor of wine
• Direct exposure to sunlight corresponds to effect of warm
  storage temperatures
• Temperature affects reaction rates involved in maturation,
  such as acceleration of hydrolysis of aromatic esters & loss
  of terpene fragrances
• Temperature can also affect wine volume & eventually
  loosen cork seal, leading to leakage, oxidation & possibly
  microbial formation resulting in spoilage of bottled wine
CRITICAL LIMITS

PROCESS STEPS   CRITICAL LIMITS

Harvesting      Rotten parts reduced to acceptable level
                Per pesticideaccording to Codex Alim.
Fermentation    As < 0.2, Cd <0.01, Cu < 1, Pb < 0.3 (mg/L)
                Pesticide residues according to Codex Alim
                Ethylene glycol & detergent residues Absent in 300 mg/L
Must            100% clean
Maturation      Absence of yeasts, molds and LAB

Stablization    As < 0.2, Cd <0.01, Cu < 1, Pb < 0.3 (mg/L)
Bottling        As < 0.2, Cd <0.01, Cu < 1, Pb< 0.3 (mg/L)
                Pesticide residues according to Codex Alim
                Absence of rifts in lute, cracks, scratches
                Yeast, LAB absence
Storage         wine quality as set by each plant
MONITORING PROCEDURES FOLLOWED

• Harvesting: Inspection during harvesting, Specific
  chemical analyses
• Fermentation: Specific chemical analyses, Gas
  chromatography
• Must: Microbiological analyses
• Maturation: Microbiological analyses
• Stabilization: Specific chemical analyses
• Bottling: Specific chemical analyses, Visual
  inspection, Sample measurements, Microbiological
  analyses
• Storage: Organoleptic controls
CORRECTIVE ACTIONS APPLIED


• Fermentation- Rejection of specific batch,
  dilution with large quantities, machinery
  modification
• Bottling- Modification of CIP, Disinfect area,
  rejection of faulty bottles
• Storage- Rejection of faulty batches
THANK
 YOU

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Implementation of hazard analysis critical control point (

  • 1. IMPLEMENTATION OF HAZARD ANALYSIS CRITICAL CONTROL POINT (HACCP) SYSTEM TO THE ALCOHOLIC BEVERAGE INDUSTRY Submitted by: Abhishek Rana Amber Awasthi Ankita Pathania Charul Sharma Deepak Dhar Devansh Jaiswal
  • 2. INTRODUCTION • Real target- minimization of unacceptable unsafe products • Prior to initiating HACCP system, company must endeavor to put together HACCP plan : a) identify HACCP resources & assemble team b) describe food & its distribution method c) state clearly intended use & consumers d) develop a process flow diagram e) verify validity of this diagram in practice (operation) • 2 most important stages- Fermentation & bottling
  • 3. HACCP Team Names of Titles/responsibilities Educational Experience or training members qualification Abhishek Rana Clean up/sanitation B. Tech (FST) _ Amber Awasthi Outside Expert B. Tech (FST) _ Ankita Pathania Laboratory, Quality B. Tech (FST) _ Assurance Charul Sharma Plant Manager B. Tech (FST) _ Deepak Dhar Production B. Tech (FST) _ Devansh Jaswal Engineer B. Tech (FST) _
  • 4. Product Description NAME OF PRODUCT RED WINE FOOD SAFETY CHARACTERISTICS pH : 3.3-3.5 Alcoholic content : 11-15% PACKAGING USED Glass bottles sealed with cork with final packaging of silver & gold paper ; bag in boxes LABELLING REQUIREMENTS Alcohol content, sulphite declaration & health warning statement STORAGE & DISTRIBUTION Store in dark, moderately humid place at 130C INTENDED CONSUMERS Adults INTENDED USE Ready to drink, as an ingredient SHELF LIFE Bottled : 2-3 years Opened (refrigerator) : 1-2 weeks
  • 5. INTENDED USE Intended use • Retail, ingredient, institutional Intended & likely consumers • Adults, elderly Distribution area • Nationwide Consumer of food • Adults (70%), elderly(20%) Distribution • Preferably refrigerated (130C)
  • 6. RED WINE • Red wine is made from dark-coloured (black) grape varieties • Actual colour range- intense violet (young wines), brick red (mature wines) & brown (older red wines) • Juice from most black grapes is greenish-white; red colour comes from anthocyanins present in the skin of the grape • Red-wine production process involves extraction of colour & flavour components from grape skin.
  • 8. PROMINENT HAZARDS IDENTIFIED • Fruit with rotten parts PHYSICAL • Bottle condition • Cork sizing • Pesticide residues • Heavy metals CHEMICAL • Residues of ethylene glycol & detergents • Methanol content • Ethyl carbamate formation • Microbial contamination of culture • Water microbiological quality MICROBIOLOGICAL • Presence of yeasts & LAB • Cork microflora
  • 9.
  • 10.
  • 11. CCP-1 (Harvesting) • Grape harvesting is CCP comprising both physical & chemical hazards • Physically, grapes should be sound without rotten parts, otherwise oxidative & microbial contamination can rapidly develop • Harvesting should be conducted with greatest possible care & efficient disease management system should be applied • Pesticides should be handled with care as they constitute chemical hazards. • At time of harvest, the grapes must have also reached correct maturity when Brix & Total Acidity levels indicate maturity of wine • Pesticide & fungicide residues on surface of berries constitute chemical hazards • Rapid & simple gas chromatography- method for determination • Maximum residue limits for pesticides (grapes & wines)- Codex Alimentarius (45) • Bulk bins used for grapes transportation, should be effectively decontaminated to avoid any microbial infection
  • 12. CCP-2 (Alcoholic Fermentation) • carried out by strains of Saccharomyces cerevisiae - grows at low pH values typical for grape must (pH 3.2–4) • chemical hazards : heavy metals presence (As<0.2, Cd<0.01, Cu<1, Pb<0.3 mg/L), methanol content (300 mg/L ), ethyl carbamate content, pesticide residues (as mentioned in the Codex Alimentarius) & residues of detergents (absence) & ethylene glycol (absence) • desirable temperature varies within the range of 25–28◦C
  • 13. CCP-3 (Must) • Possible contamination of must with killer yeasts result in stuck fermentation • Attention should be paid to added amount of SO2 i.e.175mg/L in order to inhibit
  • 14. CCP-4 (Maturation) • Maturation step often lasts 6–24 months & takes place in oak barrels • During maturation a range of physical & chemical interactions occurs among barrel, surrounding atmosphere & maturing wine, leading to transformation of flavor and composition of wine • Oak barrel should be fault-free & undergone decontamination treatment • Wood must be free of pronounced or undesirable odors, which could taint the wine • White wines are matured in oak for shorter periods than red wines & in conditioned barrels to release less extractable (tannins) • Another CCP- inhibition of O2 penetration through wood or during racking & sampling of wine • Extensive penetration can cause various sensory changes (oxidized odor, browning, loss of color in red wines, activation of spoilage bacteria & yeasts, development of ferric casse & precipitation of tannins)
  • 15. CCP-5 (Stabilization) • Reason for stabilization- production of permanently clear & flavor fault-free wine • Procedure a) tartrate stabilization by chilling wine to near its freezing point & filtering or centrifuging to remove crystals b) protein stabilization with absorption, denaturation or neutralization by fining agents (bentonite) c) polysaccharide removal with pectinases that hydrolyze polymer, disturbing its protective colloidal action & filter plugging properties d) metal casse (Fe, Cu) stabilization • Ferric casse is controlled by addition of agents (bentonites, proteins) controlling flocculation of insoluble ferric complexes • Wines with Cu content greater than 0.5 mg/L are particularly susceptible to Cu casse formation
  • 16. CCP-6 (Bottling) • Wine is bottled in glass bottles sealed with cork which must pass a decontaminating step & an inspection control to assure absence of any defects & stability of product until its consumption • Cork should be correctly sized, 6–7 mm bigger than inner neck diameter, to avoid any possible leaks • Hazards include : cork microflora, residues of heavy metals, SO2, pesticides & detergents & absence of cracks, scratches & rifts in lute • CL for cork is absence of LAB & yeast, which can be assured with microbiological analysis • For long storage of wine longer & denser corks are preferred • Headspace O2 might affect product quality by causing disease of “bottle” • CL for SO2 – 175mg/L , for As < 0.2 mg/L, Cd < 0.01 mg/L, Cu < 1 mg/L, Pb < 0.3 mg/L
  • 17. CCP-7 (Storage) • Shipping & storage of wines at elevated temperatures can initiate rapid changes in color & flavor of wine • Direct exposure to sunlight corresponds to effect of warm storage temperatures • Temperature affects reaction rates involved in maturation, such as acceleration of hydrolysis of aromatic esters & loss of terpene fragrances • Temperature can also affect wine volume & eventually loosen cork seal, leading to leakage, oxidation & possibly microbial formation resulting in spoilage of bottled wine
  • 18. CRITICAL LIMITS PROCESS STEPS CRITICAL LIMITS Harvesting Rotten parts reduced to acceptable level Per pesticideaccording to Codex Alim. Fermentation As < 0.2, Cd <0.01, Cu < 1, Pb < 0.3 (mg/L) Pesticide residues according to Codex Alim Ethylene glycol & detergent residues Absent in 300 mg/L Must 100% clean Maturation Absence of yeasts, molds and LAB Stablization As < 0.2, Cd <0.01, Cu < 1, Pb < 0.3 (mg/L) Bottling As < 0.2, Cd <0.01, Cu < 1, Pb< 0.3 (mg/L) Pesticide residues according to Codex Alim Absence of rifts in lute, cracks, scratches Yeast, LAB absence Storage wine quality as set by each plant
  • 19. MONITORING PROCEDURES FOLLOWED • Harvesting: Inspection during harvesting, Specific chemical analyses • Fermentation: Specific chemical analyses, Gas chromatography • Must: Microbiological analyses • Maturation: Microbiological analyses • Stabilization: Specific chemical analyses • Bottling: Specific chemical analyses, Visual inspection, Sample measurements, Microbiological analyses • Storage: Organoleptic controls
  • 20. CORRECTIVE ACTIONS APPLIED • Fermentation- Rejection of specific batch, dilution with large quantities, machinery modification • Bottling- Modification of CIP, Disinfect area, rejection of faulty bottles • Storage- Rejection of faulty batches