How to Write a Chemical Plant Operating Manual

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How To Write A Plant Operating ManualHow To Write A Plant Operating ManualHow To Write A Plant Operating ManualHow To Write A Plant Operating Manual
Plant Operating Manual is a guide for all the engineers who is involved in successfully
operating the plant. It is a responsibility of a process engineer working in Process Design field
to bring out the better manual which helps the operating team in start up, shutdown,
troubleshooting and optimization of the plant. Here is guidance for preparing a better plant
operating manual.
The task of writing plant manual categorized into two. One is for new plants and the other is
for plants that already running. For old plants there are already established systems and
procedures and for the modifications or revamps additional information has to be added,
which is a simple task. But writing the operating manual for new chemical plant is a
challenging task though already similar plants are running around the world. Let us will see
how to write operation manual for new plants here.
Most Process Engineers, specially the senior process engineers are required to write a plant
operating manual for a new greenfield project during their career. Mind you, this is quite
different from updating an existing operating manual for a brownfield project where the
scope of the project is modification and debottlenecking. Updation of an existing operating
manual is a simpler exercise compared to writing a new operating manual where you follow
the format of the existing operating manual and only provide an addendum to the existing
operating manual related to the scope of the project.
The real challenge lies in writing a new operating manual and that is where the experience of
the process engineer comes into fore.
In this article we have put across general guidelines on preparing a plant operating manual
based on our experience of writing a few of them. These guidelines are generic in nature and
do not subscribe to any company philosophy for writing an operating manual. These are the
basic minimum requirements to start writing an operating manual.

Note: A typical OPM would consists of the following:Note: A typical OPM would consists of the following:Note: A typical OPM would consists of the following:Note: A typical OPM would consists of the following:
Section-1: 1.Process description of the facility
2.Details of Major equipments of the facility & functioning
3.Major instrumentation & control system
Section-2: Start up ( after a major turn around/ Cold start up/Hot start up)
;includes various check list like PTW closure;Ready for start up;availability of
utilities/upstream and downstream process units etc
Section-3: Normal operations (describe operations during normal steady state
operations)
Section-4: Shut down (describe planned shut down procedures)
Section-5: Emergency shut down ( describe about various emergency like
power/utility/facility/leaks/fire etc)
Section-6: Alarms,Trips and precautions
Section-7: Interlock system (cause and effect )
Section-8: Abnormal process conditions & Trouble shooting
Section-9: Safety (includes Hazardous situation/ MSDS/process safety/ personnel
safety etc)
Section-10: Flow diagrams
Section-11: Appendix (details of equipments & tag no; safety devices;Blind list and
Isolation/deisolation procedures)

Data Collection and BrainstormingData Collection and BrainstormingData Collection and BrainstormingData Collection and Brainstorming
This is the preliminary task of a process engineer who is involved in preparation of Chemical
Plant operation manual. PFD, P& ID, Control System, Process description from Technology
provider, Equipment supplier manuals, HAZOP study recommendations, Details of legal/
regulatory requirements, Design Material & Heat balance of Process streams are to be
collected before proceeding further. Then a brainstorming session is to be arranged with the
colleagues/ superiors to discuss the various activities associated with the task and set SSSSpecific
MMMMeasurable AAAAttainable RRRRelevant TTTTime bound goal to bring up the better manual.
Following input documents and site investigations are required during preparation of
Operating Manual:
a. Basis of Design – Process Description
b. Process & Utility Flow Diagrams (PFDs and UFDs)
c. Piping & Instrument Diagrams (P&ID’s)
d. Detailed process description from "Technology Licensor" for proprietary processes if
applicable
e. Operating and Maintenance manuals of vendor equipment and packages (e.g. Instrument
Air Package, Compressor Systems, Pumps, Water Treatment Plants, Fired Heaters etc.)
f. Function logic narrative provided by Instrumentation
g. Plant Change Request
h. Management of Change
i. Interview of Site Operation Personnel
j. Interview of Site Maintenance Personnel
Contents of Chemical Plant Operating ManualContents of Chemical Plant Operating ManualContents of Chemical Plant Operating ManualContents of Chemical Plant Operating Manual
The content of a chemical plant operation manual is simplified into the following
topics and the details may be added into appropriate section based on the specific
requirements of the plant.
Abbreviations
Design Basis
Overview of the Process
Process Description
Procedures
Safety, Health & Environment Section
Utility and Other Systems
Appendix

Abbreviations and DefinitionsAbbreviations and DefinitionsAbbreviations and DefinitionsAbbreviations and Definitions
The abbreviations and definitions of terms used in the entire document are summarized
here.
Design BasisDesign BasisDesign BasisDesign Basis
Design basis of the plant including Plant Capacity, Technology used, Site Climatic Data, Raw
Materials, Utility & Product Specifications forms this section in the chemical plant operation
manual.
Overview of the ProcessOverview of the ProcessOverview of the ProcessOverview of the Process
Overview of the Manufacturing process with the major equipments or sections involved in
sequential manner to be described to get the overall understanding of the chemical plant.
Process Flow Diagram (PFD) helps in preparing this section.
Process DescriptionProcess DescriptionProcess DescriptionProcess Description
The detailed process description with Equipments and Control valves associated including tag
no’s used with the design parameters and compositions at various streams in a sequential
manner forms this section. Process control philosophy for various parameters in the plant like
pressure, flow, level & temperature and description of various controllers and control loops
available for the process control. Various Trips and Interlocks and reasons for having it along
with Emergency Shutdown (ESD) system available in that section is elaborated. Piping &
Instrumentation Diagram (P& ID) and Process description from Technology provider will be
useful in bringing effective process description of units in the chemical plant.
ProcedureProcedureProcedureProcedure:
Operating Manual is generally a Microsoft Word document. Standard operating Procedures
for individual equipment and sections in plant for Normal Operation, Start up and Shutdown
and then for total plant are to be established and produced in this section. Procedure for safe
isolation of equipment for maintenance jobs shall also be included. This section shall also
include Trouble shooting guide for various upsets. Routine schedule with incorporation of
lubrication schedule, trial run of equipment, availability check of systems etc. Equipment
supplier Manuals, HAZOP study recommendations will help the process engineer for
preparing this important section of Chemical Plant Operating manual.

StructureStructureStructureStructure:
The Operating Manual is a structured document with a particular narrative style. The
following is the sequence of the document:
- Coversheet with project title and document name i.e. Operating Manual
- 1st sheet with project title, document name i.e. Operating Manual
- List of Contents which includes:
. Abbreviations and Definitions
. Introduction which provides an overview of the project
. Process & Utility System Description
. Process Control and Automation
. Equipment Description
. Start-Up Procedure
. Normal Operating Procedure
. Shutdown Procedure
. Health, Safety & Environment (HSE)
. Appendices
IntroductionIntroductionIntroductionIntroduction:
This section provides the brief overview of the project which includes the purpose of the
facility and what it contains.
Process & Utility System DescriptionProcess & Utility System DescriptionProcess & Utility System DescriptionProcess & Utility System Description:
This section describes in detail the overall facility. The narrative should be in such a manner
that the description is in the correct sequence of the process for easy understanding. Utility
systems which supplement the main process should be described as a separate sub-section.
Wherever possible, process description should be supplemented by simple sketches showing
the major equipment and process control for a particular unit operation. This enhances the
understanding of the process.
Process Control & AutProcess Control & AutProcess Control & AutProcess Control & Automationomationomationomation:
This section provides the description of the overall controls required for the safe, reliable and
uninterrupted operation of the plant / unit. This could include flow, pressure, temperature
and level control of the plant / unit for the smooth operation of the plant / unit. Controls
required for start-up, planned shutdown and to change plant / unit capacity should be
mentioned. High and Low alarms for process operating parameters are also described in this
section.

Plant section-wise or unit-wise control systems should be addressed in a sequential manner
in order to explain the process control in continuity.
All process safety and shutdown interlocks, automation provided for emergency shutdown of
entire plant or unit of the plant should be described in this section. An example of an
emergency shutdown could be the description of the Fire and Gas Monitoring system which
initiates the plant or unit shutdown.
Tag numbers of instruments used for process control and automation should be mentioned
for sake of clarity.
Equipment DescriptionEquipment DescriptionEquipment DescriptionEquipment Description:
This section provides the functional description of the individual equipment or group of
equipment which form a unit operation in the overall context of the entire facility.
Description could include operating and design conditions for the individual equipment.
Providing tag nos. for the equipment is recommended.
Wherever possible, sketches are recommended for the sake of clarity.
StartStartStartStart----up Procedureup Procedureup Procedureup Procedure:
This section provides the description of the start-up procedure for the plant / unit under
consideration:
The first sub-section of this section should address the readiness of the plant to be started-
up. By readiness it is meant that the plant / unit is ready to accept the process or utility fluid,
raw materials or reactants. This requires that the commissioning check-lists prepared for the
plant / unit are ticked off and signed off by the start-up team. A list of the check-lists may be
provided in this section which have been signed-off to indicate readiness.
The second sub-section should address the start-up of the utility systems prior to the start-up
of the main process. Utility systems could include charging up headers for instrument air,
cooling water, inert gas for blanketing / purging etc.
The third sub-section should address the start-up of the main process. This section should
describe the valves (manual or automated) and instruments to be lined up for introducing the
process fluid (e.g. hydrocarbons, chemicals) into the equipment or equipments (e.g. piping,
vessels, tanks, reactors) of the plant / unit being started up.
Wherever applicable, reference of vendor documents for any equipment / package unit
should be provided in this section.

Normal Operating ProcedureNormal Operating ProcedureNormal Operating ProcedureNormal Operating Procedure:
This section provides the description of the normal operation of the plant / unit and indicates
the parameters to be monitored for maintaining the product quality and operational
reliability of the plant / unit.
Operating parameters should be mentioned for a particular equipment or unit or the entire
plant in this section. Sketches describing the normal operation are recommended for the
sake of clarity. Field logging and maintaining history records of critical process parameters
from the DCS or SCADA need to be mentioned in this section. Requirements of manning a
particular plant section or unit should be mentioned in this section including field monitoring
intervals by operating personnel for a particular equipment or unit.
While describing any operation it is recommended that equipment, instrument and line tag
nos. be mentioned for the sake of clarity.
Shutdown ProcedureShutdown ProcedureShutdown ProcedureShutdown Procedure:
This section provides the description of the shutdown procedures to stop the operation of
the plant.
The first sub-section of this section deals with normal shutdown due to either scheduled
maintenance and / or inspection or modification / de-bottlenecking of the plant. In this sub-
section, description should be provided for planned reduction / removal of inventory of the
process fluids from the equipment or unit to be shutdown. This would include stoppage of
fresh feed, gradual reduction of plant / unit throughput to minimise off-specification product
and final draining and purging of the equipment / unit for the purpose of complete emptying
prior to handing over for maintenance / inspection or modifications / de-bottlenecking.
The second sub-section deals with emergency shutdown procedures due to any emergency
such as an external fire, water flooding, earth quake, loss of containment of process fluid (gas
or liquid leak) etc. In this section description should be provided for the methods for isolation
of equipment or unit due to either manual initiation or automatic initiation of an emergency.
Manual initiation is emergency initiated by the operator of the plant / unit whereas
automatic initiation is emergency initiated by automatic detection of an emergency such as
detection of fire or gas leak by an automated Fire & Gas detection system.
Usage of tag nos. for equipment, valves and instruments while providing the shutdown
procedure description is recommended.
Utility and Other SystemsUtility and Other SystemsUtility and Other SystemsUtility and Other Systems

Description of various other associated facilities in Chemical Plant like Water Treatment
facility, Cooling Towers, Cooling Water system, Deaerators, Boiler & Steam System,
Compressed Air System, Inert Gas generation & distribution systems, Effluent treatment
facilities, Flare system, Electrical Power Distribution and ESD system is to be prepared and
written under this section.
Safety, Health & Environment Section:Safety, Health & Environment Section:Safety, Health & Environment Section:Safety, Health & Environment Section:
This section describes the HSE aspects of the facility that need to be considered. Safety
section provides overview of installed Safety Systems, Fire Fighting Facility and available
safety procedures in the chemical plant. It also provides details on Zone classification,
Emergency Actions, Hazards. Applicable Work permit systems related to plant like Hot Work,
Confined Space Entry and procedure for issuing and authorizing the permits are to be listed
for the entrants to understand the systems. Types of Personal Protective Equipment (PPE)
available, issue and usage details are to be provided in this section and proper sign boards
are also to be made available in plant premises.
Toxicological information of chemicals used in the manufacturing process is to be provided in
the plant operation manual. Chemical handling & storage and their first air measures also
need to be listed for better understanding of chemical hazards.
Environment section of the Plant operation manual must contain industry specific disposal
limits for various effluents generated in the plant and details on applicable laws & governing
bodies.
Health:
This sub-section relates to the health of the people and working in the plant or living in the
vicinity of the plant whose health should be a concern for the management of the plant. This
should also address the health and well being of animals and other living organisms present
in the vicinity of the plant, for e.g. marine life in any water body which would be effected by
the operations of the plant.
In this sub-section a brief description of toxicity of the chemicals used in the plant / unit,
acceptable noise levels for humans and other animals, magnitude of injuries due to fire and
explosion, first aid measures for treating injuries etc. should be provided.
Safety:
This sub-section relates to the safe start-up, operation and shutdown of the plant during its
entire lifetime. This section should address the normal hazards those are encountered in day-
to-day operations of the plant. This section should also address the safety measures available
to prevent any accident.
Some of the normal hazards could be loss of containment of any hazardous fluid due to

overflow, leak or rupture, static electricity build-up, accidental fall from heights, burns due to
exposure to hot surfaces, exposure to toxic fluids while collecting samples and piling up of
flammable solid waste (wood, paper, cloth etc.).
Description of safety measures should include:
- Special operating procedures for activities like sample collection and regular maintenance of
rotating machinery
- Issuance of work permits for hot work and vessel entry
- Usage of personal protective equipment (hard hats, safety shoes, eye goggles, ear muffs,
breathing apparatus etc.)
- Provision of field sign boards indicating the type of hazard
- Regular house-keeping
- Emergency evacuation procedures
Environment:
This sub-section describes the limits for discharge of hazardous solid, liquid and gaseous
effluents to the environment based on local laws and regulations and procedures for
compliance to them.
Appendix in Chemical Plant Operation Manual
This section contains the supporting information for better understanding of the Chemical
plant operating manual. Normally it contains PFD, P& ID, Alarm & Trip set points, MSDS of
Chemicals Handled, Equipment Data sheets & Curves, Further Reading – Vendor Document
List etc.
Process engineer can add additional resources in this section based on specific need. One can
also create his own structure based on the needs and prepare a better chemical plant
operation manual.
The appendices should preferably include the list of Process & Utility Flow Diagrams (PFDs /
UFDs), Piping & Instrument Diagrams (P&IDs), Cause and Effect Diagrams (CEDs) and
reference vendor documents, table for Alarm / Trip setpoints and lubrication schedule.
The above mentioned guidelines should help a process engineer to get started on a plant
operating manual.
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How to Write a Chemical Plant Operating Manual

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